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310 2nd Avenue South,#D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical Tnc Telephone 925 798 1620 Fax 925-798-1622 <br />' http Ilwww mcca hell corn E-mail rmin@mccarMbellcom <br /> . Advanced GeoEnvironmental,Inc Client Project ID Three B's Date Sampled 12/08/03-12/09/03 <br />' 837 Shaw Road Date Received 12/10/03 <br /> Client Contact Tun Cuellar Date Extracted 12111103-12/13/03 <br /> Stockton,CA 95215 <br />' JClient P O Date Analyzed 12/11/03-12113/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&'I and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0312190 <br />' Lab ID 0312190-005C 03 12190-006C 0312190-007C 0312190-008C <br /> Client ID MW7E MW8A ' MW8B MW8C Reporting Limit for <br /> Matrix W W W I W DF=1 <br /> rCompound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND<2 5 ND ND NA 05 <br /> t-Butyl alcohoi(TBA) ND 56 ND ND NA 50 <br /> 1,2-Dibromoethane(EDR) ND ND<2 5 ND ND NA 05 <br /> 1 2-Dichloroethane(1,2-DCA) ND ND<2 5 ND ND NA 05 <br /> • Ditsopropyl ether(DIPE) ND ND<2 5 ND ND NA 05 <br />' Ethyl tert-butyl ether(ETRE) ND ND<2 5 ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) ND 99 057 ND NA 05 <br /> `s Surrogate Recoveries(%) <br /> %SS 105 998 105 106 <br /> Comments <br /> i <br /> 'water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soiUsludge/salid samples inµglkg, wipe samples inµg/wipe, <br />' productloil/non-aqueous liquid samples in mg/1. <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> Ih)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> i <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />