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l 10 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> LA <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> I I ha//www mcc bell com E mail main@niccarripbell corn <br /> Advanced GeoEnvlronmental, Inc Client Project TD Three B's Date Sampled 12/10/03 <br /> I 837 Shaw Road Date Received 12/11/03 <br /> Client Contact Tim Cuellar Date Extracted 12/12/03 <br /> Stockton,CA 95215 <br /> [Client P O Date Analyzed 12/12/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Fxtaction Method SW5030B Analytical Method SW8260B Work Order 0312207 <br /> I Lab ID 0312207-009C 0312207-OIOC 0312207-OIIC 0312207-012C <br /> f <br /> Client ID MW12C MW12D MW12E MW12F <br /> Reporting Limit for <br /> I <br /> Matrix --_W_--- - — W----- W <br /> -- --- W DF=1 <br /> DF I — — I -I_ 1 I S W <br /> i <br /> Compound Concentration ug/kg pg/L <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 05 <br /> lie Dnsopropyl ether(DIPS) ND ND ND ND NA 05 <br /> Ethyl ter,-butyl ether IFTBE) ND ND ND I ND NA 05 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND NA 05 <br /> ISurrogate Recoveries <br /> %SS 108 107 108 107 <br /> Comments <br /> •water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soiVsludge/solid samples in gg/kg, wipe samples in gg/wipe, <br /> productloil/non-aqueous liquid samples in mg/L <br /> IND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> I h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> or anic content <br /> DHS Certification No 1644 jinAngela Rydelius, Lab Manager <br /> i <br />