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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster,PA 17605-2425•717-656-2300 Fax 717 656-2681•www lancaslertabs com <br /> Page 4 of 7 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 861384 <br /> Reported 08/11/03 at 11 35 PM - <br /> Laboratory Compliance Quality Control. <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result ML unsta REC %REC Limito RPD RPD Max <br /> Xylene (Total) N D 5 ug/1 108 84-120 _ <br /> -- -- - - - ---- - - Sample Matrix Quality Control -- -- - -- - - - - - _- - <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup <br /> RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Cone RPD Max <br /> Batch number 03213A16A Sample number(s) 4092147-4092148,4092150-4092151 <br /> TPH-GRO - Waters 110 70-130 <br /> Batch number 03213A16B Sample number(s) 4092152 <br /> TPH-GRO - Waters 110 70-130 <br /> Batch number 032151848003 Sample number(s) 4092149 <br /> Cadmium TR 104 104 78-121 0 20 N D N ❑ 0 (1) 20 <br /> Chromium TR 105 105 80-124 0 20 N D N D 0 (1) 20 <br /> Lead TR 103 104 75-125 1 20 N D N D 0 (1) 20 <br /> Nickel TR 103 103 85-116 0 20 N D N D 0 (1) 20 <br /> Zinc TR 103 102 - 80-120 " 0 20 '" N D 0 0137 24* (1) 20 <br /> Batch number 03218112601A Sample number(s) 4092148 <br /> TRPH 418 1 63 70 39-132 10 14 1 0 0 99 6 (1) 34 <br /> 0 <br /> Batch number N032211AA Sample number(s) 4092148 <br /> Ethanol 107 102 34-163 5 30 <br /> Methyl Tertiary Butyl Ether 112 110 69-134 2 30 <br /> _-di-Isopropyl_e_ther _101_ _102 75^130030 <br /> Ethyl t-butyl ether 96 97 --73-123--1-30— <br /> t-Amyl methyl ether 99 99 77-117 0 30 <br /> t-Butyl_alcohol_-_- _=�_-_111 _ _109___ 39_ <br /> _ 155_�2 - _-_30_ - - - <br /> Dichlorodifluoromethane 159 160 62-169 0 30 <br /> Chloromethane 117 126 66-142 6 30 <br /> Vinyl= Chloride = -- - -123 -134-- -64-148--m-9 — 30 - --- - - - - -- <br /> Bromomethane 125 126 46-132 1 30 <br /> Chloroethane 125 128 58-136 2 30 <br /> Trichlorofluoromethane 152 151 64-154 1 30 <br /> 1 1-Dxchloroethene 126 128 78-146 2 30 <br /> Methylene Chloride 110 111 80-126 1 30 <br /> trans-1,2-Dichloroethene 115 115 82-133 0 30 <br /> 1,1-Dichloroethane 120 118 79-135 2 30 <br /> 2,2-Dichl6ropropane 117 117 78-134 0 30 <br /> cis-1,2-Dlchloroethene 104 104 83-126 0 30 <br /> Chloroform 113 113 77-133 0 30 <br /> Bromochloromethane 96 94 55-136 3 30 <br /> 1,1,1-Trichloroethane 116 117 62-135 1 30 <br /> Carbon Tetrachloride 11B 116 73-144 2 30 <br /> 1,1-Dichloropropene 110 110 87-127 0 30 <br /> Benzene 108 107 83-128 1 30 <br /> 1,2-Dichloroethane 119 114 73-136 4 30 <br /> Trichloroethene 110 110 75-135 0 30 <br /> 1,2-Dichloropropane 99 99 81-121 0 30 <br /> Dibromomethane 107 106 83-120 1 30 <br /> Bromodichloromethane 107 107 81-127 0 30 <br /> Toluene 104 104 83-127 0 30 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ • <br /> (2) The background result was more than four times the spike added <br />