Laserfiche WebLink
® Mccampbell Analytical, Inc. 534 moxas Pass Road,PE- urg,CA 94565-1701 <br /> Web:www.mecampbell.com E-mail:main(dJnccempbell.com <br /> When Oualim Counts' I Tele hone:877-252-9262 Fac:925-252-9269 <br /> QC SUMMARY REPORT FOR E300.1 <br /> • W.O.Sample Matrix: Water QC Matrix: Water BalchlD: 38942 WorkOrder 0810383 <br /> EPA Method E300.1 Extraction E300.1 Spiked Sample ID: NIA <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/L mg/L %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> Bromide N/A 1 N/A N/A N/A 95.9 95.7 0.274 N/A N/A 85- 115 15 <br /> Chloride N/A 1 N/A N/A N/A 99.6 97.5 2.17 N/A NIA 85- 115 15 <br /> Fluoride N/A 1 N/A N/A N/A 104 104 0 N/A NIA 85- 115 15 <br /> Nitrate as N N/A I N/A N/A N/A 98.9 98.3 0.529 N/A N/A 85- 115 15 <br /> Nitrate as NO3 N/A 4.4 N/A N/A N/A 98.9 98.3 0.529 N/A N/A 85- 115 15 <br /> Nitrite as N N/A 1 N/A N/A N/A 103 102 0.389 N/A N/A 85- 115 15 <br /> Phosphate as P N/A 1 N/A N/A N/A 94.1 96.6 2.69 N/A N/A 85- 115 15 <br /> Sulfate N/A 1 N/A N/A N/A 110 108 2.23 N/A N/A 85- 115 15 <br /> ^/.SS: N/A 0.10 N/A N/A N/A 104 103 0.352 N/A N/A 90- 115 10 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 38942 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Dale Sampled Date Extracted Date Analyzed <br /> 0810383-OOIA 10/15/08 8:50 AM 10/16/08 10/16/08 9:40 PM 0810383-OOIA 10/15/08 8:50 AM 10/17/08 10/17/08 8:08 PM I <br /> 0810383-002A 10/15/08 9:50 AM 10/16/08 10/16/1 10:14 PM 0810383-002A 10/15/08 9:50 AM 10/17/08 10/17/08 2:09 PM I <br /> 0810383-002A 10/15/08 9:50 AM 10/17/08 10/17/08 8:49 PMI 0810383-003A 10/15/08 10:20 AM 10/16/08 10/16/08 10:49 PM <br /> 0810383-003A 10/15/08 10:20 AM 10/17/08 10/17/08 10:10 PMI 0810383-004A 10/15/08 11:05 AM 10/16/08 10/16/08 11:24 PM <br /> 0810383-004A 10/15/08 11:05 AM 10/17/08 10/17/08 2:44 PMI 0810383-004A 10/15/08 11:05 AM 10/17/08 10/17/08 9:29 PM I <br /> 0810383-005A 10/15/08 1:10 PM 10/16/08 10/16/08 11:58 PMI 0810383-OOSA 10/15/08 1:10 PM 10/17/08 10/17/08 6:47 PM I <br /> 0810383-006A 10/15/08 2:25 PM 10/17/08 10/17/08 12:33 AMI 0810383-006A 10/15/08 2:25 PM 10/17/08 10/17/08 3:18 PM I <br /> 0810383-006A 10/15/08 2:25 PM 10/17/08 10/17/08 7:27 PM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative percent Deviation. <br /> %Recovery=100 (MS-Sample)/(Amount Spiked):RPD=100-(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is Inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not applicable to this method. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted duetohigh matrix or analyte content.to <br /> OHS ELAP Certification 1644 — QA/QC Officer <br />