FIELD DOCUMENTS - Laserfiche WebLink

Home Browse Search

r-* McCampbell Analytical, Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 Web:www.mocampbell.00m E-mail:main@mccampbell.00m "When Oualiw Counts" I Tele hone:877-252-9262 Fax:925-252-9269 QC SUMMARY REPORT FOR E300.1 W.O.Sample Matrix: Water QC Matrix: Water BatchlD: 38830 WorkOrder 0810330 EPA Method E300.1 Extraction E300.1 Spiked Sample ID: NIA Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) ng/L mg/L %Rec. % Rec. %RPD %Rec. %Rec. %RPD MS I MSD RPD LCS/LCSD RPD Bromide N/A 1 N/A N/A N/A 93.5 93.7 0.159 N/A N/A 85- 115 15 Chloride N/A 1 N/A N/A N/A 95.1 95.1 0 N/A N/A 85- 115 IS Fluoride N/A 1 N/A N/A N/A 101 101 0 N/A N/A 85- 115 15 Nitrate as N N/A 1 N/A N/A N/A 96 96 0 N/A N/A 85- 115 IS Nitrate as NO3 N/A 4.4 N/A N/A N/A 96 96 0 N/A N/A 85- 115 15 Nitrite as N N/A 1 N/A N/A N/A 100 99.9 0.178 N/A N/A 85- 115 15 Phosphate as P N/A 1 N/A N/A N/A 93.5 93.8 0.259 N/A N/A 85- 115 15 Sulfate N/A 1 N/A N/A N/A 100 100 0 N/A N/A 85- 115 15 %SS: N/A 0.10 N/A N/A N/A 105 105 0 N/A N/A 90- 115 10 All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: NONE BATCH 38830 SUMMARY Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Dale Analyzed 0810330-OOIA 10/13/08 11:15 AM 10/14/08 10/14/08 9:30 PM 0810330-002A 10/13/08 1:10 PM 10/14/08 10/14/08 10:05 PM I 0810330-002A 10/13/08 1:10 PM 10/15/08 10/15/08 2:01 AMI 0810330-003A 10/13/08 1:10 PM 10/14/08 10/14/08 10:40 PM I 0810330-003A 10/13/08 1:10 PM 10/15/08 10/15/08 2:42 AMI 0810330-004A 10/13/08 1:30 PM 10/14/08 10/14/08 11:14 PM 0810330-004A 10/13/08 1:30 PM 10/15/08 10/15/08 3:23 AMI 0810330-OOSA 10/13/08 3:15 PM 10/14/08 10/14/08 11:49 PM 0810330-OOSA 10/13/08 3:15 PM 10/15/08 10/15/08 4:44 AMI 0810330-006A 10/13/08 3:25 PM 10/15/08 10/15/08 12:24 AM 0810330-006A 10/13/08 3:25 PM 10/15/08 10/15/08 5:25 AM MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. %Recovery=100•(MS-Sample)/(Amount Spiked);RPD=100•(MS- MSD)/((MS+MSD)/2). MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. N/A=not applicable to this method. NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. OHS ELAP Certification 1644 QA/QC Officer