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McCamubell Analytical. IDC. 1534 Willow Pam Road,Pimburg,CA 94565-1701 <br /> Web:www.mccampbell.com &mail:main@mccampbell.com <br /> When Quality Counts" Telephone:877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR E200.8 <br /> ow 0.Sample Matrix: Water QC Matrix: Water BatchlD:38864 WorkOrder: 0810330 <br /> EPA Method: E200.8 Extraction: E200.8 Spiked Sample ID: 0810226-001F <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> pg/L pg/L %Rec. %Rec. %RPD %RealMS/MSD RPD LCS/LCSD RPD <br /> Calcium 2500 1000 92 89.3 0.792 10670-130 20 70-130 20 <br /> Magnesium 300 100 88 92.7 1.21 10870-130 20 70-130 20 <br /> Potassium 12,000 100 NR NR NR 81.770-130 20 70-130 20 <br /> Sodium 2,200,000 1000 NR NR NR 10770-130 20 70-130 20 <br /> %55: 99750 98 96 1.93 9970-130 20 70-130 1 20 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 38864 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0810330-OOID 10/13/08 11:15 AM 10/14/08 10/16/08 3:50 PM 0810330-OOID 10/13/08 11:15 AM 10/14/08 10/16/08 5:11 PM <br /> 0810330-004D 10/13/08 1:30 PM 10/14/08 10/16/08 3:58 PM 0810330-005D 10/13/08 3:15 PM 10/14/08 10/16/08 4:06 PM <br /> 0810330-006D 10/13/08 3:25 PM 10/14/08 10/16/08 4:38 PM <br /> 0 <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or mom,of the following reasons:a)the sample is inhomogenous AND contains <br /> significant concentrations of analyte relative M the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not applicable to this method. <br /> NR=matrix interference and/or analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix <br /> or analyte content <br /> OHS ELAP Certification 1644 4w QA/QC Officer <br />