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Scgnoi a $85 Jarvis037 <br /> iA Morgan Hill CAA95037 <br /> 4 (408)°77&9600 <br /> 4X-1 <br /> Analytical FAX(408)782-6308 <br /> Blame Tech Services(Shell) Project 3725 South Tracy Blvd <br /> 1680 Rogers Avenue Project Number 000501-K1 Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 05/19/00 13 43 <br /> MTBE by EPA Method 8260A - Quality Control <br /> Sequoia Analytical- Morgan Hill <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch OE09007- EPA 5030B PIT] <br /> Blank(OE09007-BLKI) Prepared&Analyzed 05/08/00 <br /> Methyl tert-butyl ether ND too ugtl <br /> Surrogate 12-Dichloroethane-d4 949 100 949 70-130 <br /> LCS(OE09007-BS1) Prepared&Analyzed 05/08/00 <br /> Methyl tert-butyl ether 8 11 100 ug/l 100 811 70-130 <br /> Surrogate 12-Drchloroethane-d4 945 11100 945 70-130 <br /> Matrix Spike(OE09007-MSI) Source MJD0789-01 Prepared&Analyzed 05/08/00 <br /> Methyl tett-butyl ether 466 200 ug/l 200 304 810 70-130 _ <br /> Surrogate 12-Dichloroethane-d4 956 11100 956 70-130 <br /> Matrix Spike Dup(OE09007-MSDI) _'_ Source- MJD0789-01 Prepared&Analyzed 05108/00 __ _ <br /> Methyl tert-butyl ether 455 200 ugll 200 304_ 755 70-130 239 25 <br /> Surrogate 1 1-Drchloroeihane-d4 980 100 980 70-130 <br /> etch OE10006-EPA 5030B IPfFI <br /> = Blank(OE10006=BLK1) _ Prepared&Analyzed 05/08/00 <br /> Methyl tert-butyl ether ND 100 ug/1 <br /> -Surrogate 12-Drchloroethane=d4-=- - -9 85------ - =- 100 --- --=98 5 —70-130_ - <br /> LCS(OE10006-BSI)__-- ­ Prepared&Analyzed 05/08/00 - <br /> Methyl tert-butyl ether �8 11 �$ 100 ugfl 100 81 1 70-130 <br /> Surrogate 12-Dichloroethane-d4 967 11 100 967 10-130 <br /> Matrix Spike(OE10006-MSI) Source MJD0791-03 Prepared&Analyzed 05/08/00 <br /> Methyl tert-butyl ether 3610 200 ugll 2000 1940 83 5 70-130 <br /> Surrogate 1 2-Dichloroethane-d4 108 too t os 70-130 <br /> I <br /> Sequoia Analytical-Morgan Hill The results in this report apply to the samples analyzed in accordance wrth the c <br /> custody document This analytical report must he reproduced in its en <br /> Page 8 of 10 <br />