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1 <br />' 4 McCampbell Analytical, Inc. 'l0 2lephonend c 25 79#16 Pacheco 25 99 16 5560 <br /> Telephone 925 798 1620 Fax 925 798 1622 <br /> Website www mccampbell com E-mail mam@mecampbell com <br /> E:Port of Stockton Client Project ID Port of Stockton UST Date Sampled 06/01/05 <br /> Site No 3 <br /> P O Box 2089 Date Received 06/03/05 <br /> Stockton,CA 95201-2089 Client Contact Ruta Koehnen Date Extracted 06/07/05 <br /> Client P O Date Analyzed 06/07/05 <br /> Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline'' <br /> Extraction method SW5030B Analytical methods SW801SCm Work Order 0506068 <br /> Lab ID Client ID Matrix TPH(g) DF %SS <br />' 001A MW 3-1 W 170 a ] 102 <br /> 002A MW 3-2 W 2300 a 1 109 <br /> 003A MW 3-3 W 2300,a 1 109 <br /> 004A MW 3-4 W ND 1 93 <br />' 005A MW 3-5 W ND 1 94 <br /> 006A MW 3-6 W 2800,a 10 106 <br /> 1 007A Trip Blank W ND 1 98 <br /> t <br /> Reporting Limit for DF=1 'W 50 AWL <br /> ND means not detected at or <br /> above the reporting limit S NA NA <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludge/solid samples in mg/kg wipe samples in gg/wipe, <br />' product/oll/non-aqueous liquid samples in mg/L <br /> #cluttered chromatogram sample peak coelutes with surrogate peak <br /> +The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation a) <br />' unmodified or weakly modified gasoline is significant b)heavier gasoline range compounds are significant(aged gasolme?) c)lighter gasoline range <br /> compounds(the most mobile fraction)are significant,d)gasoline range compounds having broad chromatographic peaks are significant biologically <br /> altered gasoline?,e)TPH pattern that does not appear to be derived from gasoline(stoddard solvent/mineral spirit?) f)one to a few isolated non-target <br /> peaks present,g)strongly aged gasoline or diesel range compounds are significant,h)lighter than water immiscible sheen/product is present i)liquid <br />' sample that contains greater than—1 vol %sediment 3)reporting limit raised due to high MTBE content k)TPH pattern that does not appear to be <br /> derived from gasoline(aviation gas) m)no recognizable pattern,n)TPH(g)range non-target isolated peaks subtracted out ofthe TPH(g)concentration at <br /> the client's request <br />' DHS Certification No 1644 Angela Rydellus,Lab Manager <br />