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PRTUMOH WRONG CERTIFICATE OFANALYSIS <br /> Analytical Laboratory <br /> 3935 N.Coronado Ave,Stockton CA.95204 Phone:(209)477-8105 <br /> Associated Tractor Service,Inc Project Number: Clean Up <br /> 1323 W.Chater Way Project Name: Clean Up Work Order No.: <br /> Stockton,CA 95206 <br /> Project Manager. Larry Borell <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Reporting Spike Source <br /> Analyte Result Limit Units Level Result %REC RPD Notes <br /> Blank(AC01001-BLK1) <br /> Surrogate:DibromoJluoromethane 19.2 ug/kg 25.0 77 70-125 <br /> tert-Butyl Alcohol(TBA) ND 50.0 <br /> Methyl tert-butyl Ether(MtBE) ND 5.00 <br /> Diisopropyl Ether(DIPE) ND 5.00 <br /> Ethyl tert-Butyl Ether(ETBE) ND 5.00 <br /> tert-Amyl Methyl Ether(TAME) ND 5.00 <br /> 1,2-Dibromoethane(EDB) ND 5.00 <br /> 1,2-Dichloroethane ND 5.00 <br /> Ethylbenzene ND 5.00 <br /> Benzene ND 5.00 " <br /> Toluene ND 5.00 <br /> m,p-Xylene ND 5.00 <br /> o-Xylene ND 5.00 <br /> TPH-Gasoline ND 200 <br /> LCS(AC01001-BS1) <br /> Surrogate:DibromoJluoromethane 25.9 ug/kg 25.0 104 70-125 <br /> Ethylbenzene 33.8 5.00 34.0 99 <br /> Benzene 21.1 5.00 20.8 102 <br /> Toluene 160 5.00 160 100 <br /> m,p-Xylene 135 5.00 136 99 <br /> o-Xylene 53.1 5.00 52.8 100 <br /> TPH-Gasoline 2320 200 2220 105 <br /> LCS Dup(AC01001-BSDI) <br /> Surrogate:Dibromofluoromethane 26.6 ug/kg 25.0 106 70-125 <br /> Ethylbenzene 33.2 5.00 34.0 98 2 <br /> Benzene 21.2 5.00 20.8 102 0.4 <br /> Toluene 160 5.00 160 100 0.1 <br /> m,p-Xylene 134 5.00 136 99 0.5 <br /> o-Xylene 51.0 5.00 52.8 97 4 <br /> TPH-Gasoline 2320 200 2220 105 0.09 <br /> Matrix Spike(AC01001-MS1) <br /> Surrogate:DibromoJluoromethane 26.0 ug/kg 25.0 104 70-125 <br /> (�4/4w� <br /> Approved By <br /> Precision Enviro-Tech. - California D.O.H.S.Cert.#2387 <br /> Page 9 of 12 <br />