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GeoAnalytical Laboratories, Inc. 1405 Kansas Avenue Modesto CA 95351 Certification#2585 Phone(209)572-0900 Fax(209)572-0916 Report# T7L2804 Project: . Date: 01/09/08 San Joaquin County Environmental Health Date Recd: 12/28/07 600 East Main St PO#: Stockton,CA 95202 Inorganic Chemistry-Quality Control GeoAnalytical Laboratories, Inc. Reporting Spike Source %REC RPD nalvte Result Limit Units Level Result %RLC Limits RPD Limit Notes Batch U000011 -3050B Prepared: 01/07/08 Analyzed: 01/08/08 LCS Dup(0000011-BSD1) Antimony 5.36 0.5 mg/kg 5.000 107 80-120 4 20 Arsenic 5.22 0.5 5.000 104 80-120 8 20 Barium 12.4 0.5 12.50 99 80-120 3 20 Beryllium 5.28 0.5 5.000 106 80-120 1 20 Cadmium 5.23 0.5 5.000 105 80-120 4 20 Chromium 4.88 0.5 5.000 98 80-120 10 20 Cobalt 5.54 0.5 5.000 111 80-120 5 20 Copper 5.95 0.5 5.000 119 80-120 0.2 20 Lead 5.10 1.0 5.000 102 80-120 1 20 Molybdenum 5.69 0.5 5.000 114 80-120 4 20 Nickel 5.60 0.5 5.000 112 80-120 5 20 Selenium 5.90 0.5 5.000 118 80-120 8 20 Silver 49.0 10 50.00 98 80-120 6 20 Thallium 4.71 0.5 5.000 94 80-120 1 20 Vanadium 12.2 0.5 12.50 98 80-120 8 20 Zinc 5.98 0.5 5.000 120 80-120 7 20 Mercury 1.30 0.5 1.250 104 80-120 1 20 Matrix Spike(U000011-MSI) Source:T7L2804-01 Antimony 2.79 0.5 mg/kg 5.000 ND 56 80-120 QM-01 Arsenic 10.8 0.5 5.000 5.28 Ill 80-120 Barium 193 0.5 12.50 143 397 80-120 QM-02 Beryllium 5.61 0.5 5.000 ND 112 80-120 Cadmium 5.84 0.5 5.000 ND 117 80-120 Chromium 33.6 0.5 5.000 22.9 215 80-120 QM-02 Cobalt 15.4 0.5 5.000 9.45 118 80-120 Copper 35.2 0.5 5.000 24.6 213 80-120 QM-02 Lead 63.1 1.0 5.000 30.5 652 80-120 QM-02 Molybdenum 5.93 0.5 5.000 ND 119 80-120 Nickel 29.7 0.5 5.000 22.0 155 80-120 QM-02 Selenium 4.60 0.5 5.000 0.90 74 80-120 QM-01 Silver 63.9 1.0 50.00 ND 128 80-120 QM-01 Thallium 4.88 0.5 5.000 ND 98 80-120 Vanadium 52.8 0.5 12.50 38.3 116 80-120 Zinc 121 0.5 5.000 79.2 839 80-120 QM-02 Mercury 1.02 0.5 1.250 ND 82 80-120