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a Laboratories Inc. I. WL---- <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107.03 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> BCL Sample ID: 1218782-01 Client Sample Name: Diamond Pet, 013-1, 10/2/2012 10:07:OOAM, David Kirk <br /> MB Lab <br /> Constituent Result Units PQL MDL Method Bias Quals Run # <br /> Dissolved Calcium 110 mg/L 0.10 0.018 EPA-200.7 ND <br /> Dissolved Magnesium 41 mg/L 0.050 0.016 EPA-200.7 ND <br /> Dissolved Sodium 220 mg/L 0.50 0.050 EPA-200.7 ND <br /> Dissolved Potassium 7.2 mg/L _ 1.0 0.10 EPA-200.7 ND i <br /> Bicarbonate 670 mg/L 10 10 EPA-310.1 ND 2 <br /> Carbonate ND mg1L 5.0 5.0 EPA-310.1 ND 2 <br /> Alkalinity as CaCO3 550 mg1L 8.2 8.2 Calc ND 3 <br /> Chloride 140 mg/L 0.50 0.066 EPA-300.0 ND 4 <br /> Nitrate as N 31 mg/L 0.20 0.042 EPA-300.0 ND A01 5 <br /> Sulfate 100 mg/L 1.0 0.12 EPA-300.0 ND 4 <br /> Dissolved Hardness as CaCO3 450 mg/L 0.50 0.10 Calc ND 3 <br /> PH 7.27 pH Units 0.05 0.05 EPA-150.1 S05 6 <br /> Electrical Conductivity @ 25 C 1570 umhoslc 1.00 1.00 EPA-120.1 - 7 <br /> m <br /> Total Dissolved Solids @ 180 C 1100 mg/L 50 50 EPA-160.1 ND $ <br /> Total Nitrogen -F 31 mg/L 0.60 0.20 Calc ND 9 <br /> Total Kjeldahl Nitrogen 0.091 mg/L 0.20 0.056 EPA-351.2 ND J _ 10- <br /> Run QC <br /> Run# Method Prep Date Date/Time Analyst Instrument Dilution Batch ID <br /> 1 EPA-200.7 10/03/12 10/05/12 13:39 JRG PE-0172 1 BVJ0505 <br /> 2 EPA-310.1 10/05/12 10/05/12 09:43 RML MET-1 2 BVJ0435 <br /> 3 Calc 10/05/12 - 10/15/12 15:51 TMS Calc 1 BVJ0487 <br /> 4 EPA-300.0 10/03/12 10/04/12 00:45 LS1 IC2 1 BVJ0293 <br /> 5 EPA-300.0 10/03/12 10/03/12 16:21 LS1 IC2 2 BVJ0293 <br /> 6 EPA-150.1 10/05/12 10/05/12 09:43 RML MET-1 1 BVJ0435 <br /> 7 -EPA-120.1 10/05/12 10/05/12 09:43 RML MET-1 1 BVJ0435 <br /> 8 EPA-160.1 10/05/12 10/05/12 08:50 NW1 MANUAL 5 BVJ0444 <br /> 9 Calc 10105/12 10/15/12 15:53 TMS Calc 1 BVJ0487 <br /> 10 EPA-351.2 10/12/12 10/15/12 90:42 SDU SC-1 1 BVJ1085 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety, <br /> All results listed in this report are for the exclusi-se use of the submitting party BC Laboratories,Inc.assumes no responsibility for report alteratioty separation,detachment or third parry interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 16 of 60 <br />