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14ALLaboratories Inc. <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107,03 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> BCL Sample ID: 1218782-03 Client Sample Name: Diamond Pet, 013-4, 10/2/2012 12:17:OOPM, David Kirk <br /> MB Lab <br /> Constituent Result Units PQL MDL Method Bias Quals Run # <br /> Dissolved Calcium 180 mg/L 0.10 0.016 EPA-200.7 NO <br /> Dissolved Magnesium 65 mg/L 0.050 0.016 EPA-200.7 NO <br /> Dissolved Sodium 380 mg/L 0.50 0.050 EPA-200.7 NO <br /> Dissolved Potassium 13 mg/L 1.0 0.10 EPA-200.7 ND 1 <br /> Bicarbonate 940 - mg/L 10 10 EPA-310.1 ND 2 <br /> Carbonate ND mg/L 5.0 5.0 EPA-310.1 NO 2 <br /> Alkalinity as CaCO3 770 mg/L 8.2 8.2 Calc NO 3 <br /> Chloride 360 mg/L 1.0 0.13 EPA-300.0 NO A01 4 <br /> Nitrate as N 0.21 mg/L 0.20 0.042 EPA-300.0 NO A01 4 <br /> Sulfate 290 mg/L 2.0 0.24 EPA-300.0 NO A01 4 <br /> Dissolved Hardness as CaCO3 710 mglL 0.50 0.10 Calc NO 3 <br /> PH 7.33 pH Units 0.05 0.05 EPA-150.1 S05 5 <br /> Electrical Conductivity @ 25 C 2720 umhos/c 1.00 --1.00 EPA-120.1 6 <br /> m <br /> Total Dissolved Solids @ 180 C 1900 mg/L 100 100 EPA-160.1 NO 7 <br /> Total Nitrogen - 2.2 mg/L 0.60 - 0.20 Cale ND <br /> Total Kjeldahl Nitrogen - 2.0 T mg/L 0.20 0.056 EPA-351.2 NO - -- 9 <br /> Run QC <br /> Run# Method Prop Date Datel7ime Analyst Instrument Dilution Batch ID <br /> 1 EPA-200.7 10/03/12 10/05/12 13:54 JRG PE-OP2 1 BVJ0505 <br /> 2 EPA-310.1 10/05/12 10/05/12 10:10 RML MET-1 2 BVJ0436 <br /> 3 Calc 10/05/12 10/15/12 15:51 TMSmm Calc 1 BVJ0487 <br /> 4 EPA-300.0 10/03/12 10/04/12 04:22 LD1 - IC2 2 BVJ0293 <br /> 5 EPA-150.1 10/05/12 10/05/12 10:10 RML META 1 BVJ0436 <br /> 6 EPA-120.1 10/05/12 10/05/12 10:10 RML -- MET-1 1 BVJ0436 <br /> 7 EPA-160.1 10/05/12 10/05/12 08:50 NW1 MANUAL 10 BVJ0444 <br /> 8 Calc 10/05/12 10/15/12 15:53 TMS Calc 1 BVJ0487 <br /> 9 EPA-351.2 10/12/12 10/15/12 10:46 SDU SC-1 1 BVJ10B5 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party BC Laboratories.Inc.assumes no responsibility for report alteration separation,detachment or third parry interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 20 of 60 <br />