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:W Laboratories Inc. 1�.W <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107.03 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> BCL Sample ID: 1218782-05 Client Sample Name: Diamond Pet, OB-7, 10/2/2012 12:07:QQPM, David Kirk <br /> MB Lab <br /> Constituent Result Units PQL MDL Method Bias Quals Run# <br /> Dissolved Calcium 58 mg/L 0.10 0.018 EPA-200.7 ND 1 <br /> Dissolved Magnesium 17 mg/L 0.050 0.016 EPA-200.7 ND 1 <br /> Dissolved Sodium -- 130 mg/L 0.50 0.050 EPA-200.7 ND 1 <br /> Dissolved Potassium 2.4 mg/L 1.0 0.10 EPA-200.7 ND 1 <br /> Bicarbonate 340 mg/L 5.0 5.0 EPA-310.1 ND 2 <br /> Carbonate ND mglL 2.5 2.5 EPA-310.1 ND 2 <br /> Alkalinity as CaCO3 - 260 mg/L 4.1 4.1 Calc ND 3 <br /> Chloride 60 mg/L 0.50 0.066 EPA-300.0 ND 4 <br /> Nitrate as N 12 - mg1L 0.10 0.021 EPA-300.0 ND <br /> Sulfate 92 mg/L 1.0 0.12 EPA-300.0 ND 4 <br /> Dissolved Hardness as CaCO3 210 mg/L 0.50 0.10 Calc ND 3 <br /> pH 7.51 pH Units 0.05 0.05 EPA-150.1 S05 5 <br /> Electrical Conductivity @ 25 C 934 umhos/c 1.00 1.00 EPA-120.1 6 <br /> M <br /> Total Dissolved Solids @ 180 C 660 mg/L 33 33 EPA-160.1 ND 7 <br /> Total Nitrogen - -12 mg/L 0,30 0.10 Calc ND <br /> Total Kjeldahl Nitrogen 0.39 mg/L 0.20 0.056 EPA-351.2 ND -9 <br /> - <br /> Run QC <br /> Run# Method Prep Date Date/Time Analyst Instrument Dilution Batch ID <br /> 1 EPA-200.7 10/03/12 10/05/12 14:06 JRG PE-0132 1 BVJ0505 <br /> 2 EPA-310.1 10/05/12 10/05/12 10:30 RML MET-1 1 BVJ0436 <br /> 3 Calc 10/05/12 10/15/12 15:51 TMS Calc 1 BVJ0487 <br /> 4 - EPA-300.0 10/03/12 10/03/12 17:15 LS1 IC2 1 BVJ0293 <br /> 5 EPA-150.1 10/05/12 10/05/12 10:30 RML MET-1 1 BVJ0436 <br /> 6 EPA-120.1 10/05/12 10/05/12 10:30 RML META 1 BVJ0436 <br /> 7 EPA-160.1 10/05/12 10/05/12 08:50 NW1 MANUAL 3.333 BVJ0444 <br /> y 8 Calc 10/05/12 10/15/12 15:53 TMS Calc 1 BVJ0487 <br /> 9 EPA-351.2 10/12/12 10/15/12 10:48 SDU SC-1 1 BVJ1085 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party BC Laboratories,Inc.assumes no responsibility for report alteratiory separation,detachment or third party interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bc[abs.com Page 24 of 60 <br />