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Laboratories, Inc. ji,�Environmental Testing Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107.03 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> BCL Sample ID: 1218782-07 Client Sample Name: Diamond Pet, OB-11, 10/2/2012 10:21:OOAM, David Kirk <br /> MB Lab <br /> Constituent Result Units PQL MDL Method Bias Qualls Run# <br /> Dissolved Calcium 110 mg/L 0.10 0.018 EPA-200.7 ND 1 <br /> Dissolved Magnesium 42 v mg/L 0.050 0.016 EPA-200.7 ND 1 <br /> Dissolved Sodium 170 mg1L 0.50 0.050 EPA-200.7 ND <br /> Dissolved Potassium 4.3 mg1L 1.0 0.10 EPA-200.7 ND 1 <br /> Bicarbonate 620 T mg/L 10 - 10 EPA-310.1. ND 2 <br /> Carbonate ND mg/L 5.0 5.0 EPA-310.1 ND 2 <br /> Alkalinity as CaCO3 510 mg1L 8.2 8.2 Calc ND _ - 3 <br /> Chloride 250 mg/L 1.0 0.13 EPA-300.0 ND A01 4 <br /> Nitrate as N 0.67 mg1L 0.20 0.042 EPA-300.0 ND A01 4 <br /> Sulfate 16 mg1L 2.0 0.24 EPA-300.0 ND A01 4 <br /> Dissolved Hardness as CaCO3 450 - mg1L 0.50 0.10 Calc ND 3 <br /> pH 6.59 pH Units 0.05 0.05 EPA-150.1 S05 5 <br /> Electrical Conductivity @ 25 C 1590 umhoslc 1.00 1.00 EPA-120.1 6 <br /> m <br /> Total Dissolved Solids @ 180 C 1000 mg/L 50 50 EPA-160.1 ND 7 <br /> Total Nitrogen 1.7 mg11- 0.60 0.20 Calc ND - -- _ 8 <br /> Total Kjeldahl Nitrogen 1.1 mg1L 0.20 0.056 EPA-351.2 ND 9 <br /> Run QC <br /> Run# Method Prop Date DatelTime Analyst Instrument Dilution Batch ID <br /> 1 EPA-200.7 10/03/12 10/05/12 14:11 JRG PE-OP2 1 BVJ0505 <br /> 2 EPA-310.1 10/05/12 10/05/12 10:43 RML MET-1 2 BVJ0436 <br /> 3 Calc 10/05/12 10/15/12 15:52 TMS Calc 1 BVJ0487 <br /> 4 EPA-300.0 10/03/12 10/03/12 17:42 LS1 IC2 2 BVJ0293 <br /> 5 EPA-150.1 10/05/12 10105/12 10:43 RML - MET-1 _ _ 1 - BVJ0436 - T <br /> 6 EPA-120.1 10/05/12 10/05/12 10:43 RML MET-1 1 BVJ0436 <br /> 7 TEPA-160.1 10105!12 10/05/12 08:50 NW1 -- MANUAL 5 BVJ0444 <br /> 8 Calc 10/05/12 10/15/12 15:53 TMS Calc 1 BVJ0487 <br /> 9 EPA-351.2 10/12/12 10/15/12 10:49 SDU - SC-1 1 BVJ1085 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party BC Laboratories,Inc.assumes no responsibility for report alteration separation,detachment or third patty interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)3274911 FAX(661)327-1918 www.bclabs.com Page 28 of 60 <br />