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i11 <br /> _Laboratories, Inc. N n I - <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107.03 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> BCI_Sample ID: 1218782-09 Client Sample Name: Diamond Pet, OB-19, 10/2/2012 8:42:OOAM, David Kirk <br /> MB Lab <br /> Constituent Result Units PQL MDL Method Bias Qualls Run# <br /> Dissolved Calcium 91 mg/L 0.10 0.018 EPA-200.7 ND 1 <br /> Dissolved Magnesium 17 mg/L 0.050 0.016 EPA-200.7 ND 1 <br /> Dissolved Sodium 110 mglL 0.50 0.050 EPA-200.7 ND <br /> Dissolved Potassium 4.2 mg/L 1.0 0.10 EPA-200.7 ND <br /> Bicarbonate 340 -- mg/L 5.0 -�5.0 EPA-310.1 ND 2 <br /> Carbonate ND mg/L 2,5 2.5 EPA-310.1 ND 2 <br /> Alkalinity as CaCO3 280 mg/L 4.1- -� 4.1 Calc ND 3 <br /> Chloride 64 - mg/L 0.50 0.066 EPA-300.0 ND 4 <br /> Nitrate as N 15 mg/L 0.10 0.021 EPA-300.0 ND 4 <br /> Sulfate 94 mg/L 1.0 0.12 EPA-300.0 ND 4 <br /> Dissolved Hardness as CaCO3 300 mg/L 0.50 0.10 Calc ND 3 <br /> PH 7.37 pH Units 0.05 _ 0.05 EPA-150.1 505 5 <br /> Electrical Conductivity @ 25 C 993 umhos/c 1.00 1.00 EPA-120.1 6 <br /> m <br /> Total Dissolved Solids @ 180 C 730 mg/L 33 33 EPA-160.1 ND 7 <br /> Total Nitrogen 16 mg/L 0.30 0.10 Cale ND 8 <br /> Total Kjeldahl Nitrogen 0.42 mg/L 0.20 0.056 EPA-351.2 ND 9 <br /> Run QC <br /> Run# Method Prep Date Date/Time Analyst Instrument Dilution Batch ID <br /> 1 EPA-200.7 10/03/12 10/05/12 14:16 JRG PE-OP2 1 BVJ0505 <br /> 2 EPA-310.1 10/05/12 10/05/12 10:55 RML MET-1 1 BVJ0436 <br /> 3 Calc 10/05/12 10/15/12 15:52 TMS - Calc 1 BVJ0487 <br /> 4 EPA-300.0 10/03/12 10/03/12 18:10 LS1 IC2 1 BVJ0293 <br /> 5 EPA-150.1 10/05/12 10/05/12 10:55 RML MET-1 1 BVJ0436 <br /> 6 EPA-120.1 10/05/12 10/05/12 10:55 RML MET-1 1 BVJ0436 <br /> 7 EPA-160.1 10/05/12 10/05/12 08:50 NW1 MANUAL 3.333 BVJD444 <br /> 8 Calc 10/05/12 10/15/12 15:53 TMS Calc 1 BVJ0487 <br /> 9 EPA-351.2 10/12/12 10/15/12 11:01 SDU SC-1 1 BVJ1086 <br /> The results in this report apply to the samples analysed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br /> All results listed in this report are far the exclusive use of the submitting party 9C Laboratories,Inc.assumes no responsibility for report alteratiort separation,detachment or third parry interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 32 of 60 <br />