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� <br /> Laboratories9Inc. 1i!ii , <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107.03 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> BCL Sample ID: 1218782-13 Client Sample Name: Diamond Pet, OB-25, 10/2/2012 1:08:OOPM, David Kirk <br /> MB Lab <br /> Constituent Result Units PQL MDL Method Bias Quals Run# <br /> Dissolved Calcium 130 mglL 0.10 0.018 EPA-200.7 ND <br /> Dissolved Magnesium 67 mg1L 0.050 0.016 EPA-200.7 ND <br /> Dissolved Sodium 130 mglL 0.50 0.050 EPA-200.7 0.090 1 <br /> Dissolved Potassium 3.3 mglL 1.0 0.10 EPA-200.7 ND <br /> Bicarbonate 360 mglL 10 10 EPA-310.1 ND 2 <br /> Carbonate ND mg1L 5.0 5.0 EPA-310.1 ND 2 <br /> Alkalinity as CaCO3 300 mglL 8.2 8.2 Calc ND 3 <br /> Chloride 260 mglL 1.0 0.13 EPA-300.0 ND A01 4 <br /> Nitrate as N 3.8 mg/L 0.20 0.042 EPA-300.0 ND A01 4 <br /> Sulfate 210 mglL- 2.0 0.24 EPA-300.0 ND A01 4 <br /> Dissolved Hardness as CaCO3 600 _ mglL 0.50 0.10- Calc ND 3 <br /> pH - - - - - 7.29 pH Units 0.05 0.05_ EPA-150.1 S05 5 <br /> Electrical Conductivity @ 25 C 1600 umhoslc 1.00 1.00 EPA-120.1 6 <br /> m <br /> Total Dissolved Solids @ 180 C 1100 m 1L 5o 50 EPA-160.1 ND 7 <br /> Total Nitrogen 4.3 mg/L ' 0.60 0.20 Calc ND 8 <br /> Total Kjeldahl Nitrogen- -� 0.52 mg/L 0.20 0.056 EPA-351.2 ND 9 <br /> Run QC <br /> Run# Method Prep Date Date/Time Analyst Instrument Dilution Batch ID <br /> 1 EPA-200.7 10/03/12 10/05/12 14:46 JRG PE-OP2 1 BVJ0506 <br /> 2 EPA-310.1 10/05/12 10/05/12 12:30 RML MET-1 2 BVJ0437 <br /> 3 Calc 10/05/12- 10/15/12 15:52 TMS Calc 1 BVJ0487 <br /> 4 EPA-300.0 10/03/12 10/03/12 19:31 LS1 IC2 2 BVJ0294 <br /> 5 EPA-150.1 10/05/12 10/05/12 12:30 RML MET-1 1 BVJ0437 <br /> .._..._. ....... <br /> 6 E=PA-120.1 10/05/12 10/05/12 12:30 RML MET-1 1 BVJ0437 <br /> 7 EPA-160.1 10/05/12 10/05/12 09:25 NW1 MANUAL 5 BVJ0445 <br /> 8 Calc 10/05/12 10/15/12 15:53 TMS Calc 1 BVJ0487 <br /> 9 EPA-351.2 10/12/12 10/15/12 11.06 5DU SC-1 1 BVJ1086 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party BC Laboratories,Inc.assumes no responsibility for report alteration separation,detachment or third party interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(651)327-1918 www.bclabs.com Page 40 of 60 <br />