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Laboratories, Inc. <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107.03 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> BCL Sample ID: 1218782-16 Client Sample Name: Diamond Pet, PW-6, 10/2/2012 10:50:00AM, David Kirk <br /> MB Lab <br /> Constituent Result Units PQL MDL Method Bias Quals Run # <br /> Dissolved Calcium 19 mglL 0.10 0.018 EPA-200.7 NO 1 <br /> Dissolved Magnesium 5.3 mg/L 0.050 0.016 EPA-200.7 ND 1 <br /> Dissolved Sodium 64 mg/L 0.50 0.050 EPA-200.7 0.090 1 <br /> Dissolved Potassium 3.4 mg/L 1.0 0.10 EPA-200.7 ND 1 <br /> Bicarbonate 180 mg/L 5.0 5.0 EPA-310.1 ND 2 <br /> Carbonate ND mg1L 2.5 2.5 EPA-310.1 ND 2 <br /> Alkalinity as CaCO3 150 mg/L 4.1 4.1 Calc ND _ 3 - <br /> Chloride 15 mg/L 0.50 0.066 EPA-300.0 ND 4 <br /> Nitrate as N 3.3 mg/L 0.10 0.029 EPA-300.0 NO 4 <br /> Sulfate 25 mg/L 1.0 0.12 EPA-300.0 ND 4 <br /> Dissolved Hardness as CaCO3 69 mg/L 0.50 0.10 Calc ND 3 <br /> pH 7.96 pH Units 0.05 0.05 EPA-150.1 S05 6 <br /> Electrical Conductivity @ 25 C 399 - umhoslc 1.00 1.00 EPA-120.1 6 <br /> _ m <br /> Total Dissolved Solids @ 180 C 300 - mg/L - 20 -20 EPA-160.1 ND 7 <br /> Total Nitrogen 3.3 mg/L 0.30 0.10 Calc ND 8 <br /> Total Kjeldahl Nitrogen ND mg/L 0.20 0.056 EPA-351.2 ND 9 <br /> Run CC <br /> Run# Method Prep Date Date/Time Analyst instrument Dilution Batch ID <br /> 1 EPA-200.7 10/03/12 10/05/12 14:59 JRG PE-OP2 1 BVJ0506 <br /> 2 EPA-310.1 10/05/12 10/05/12 12:54 RML MET-1 1 BVJ0437 - -- <br /> 3 Calc 10/05/12 10/15/12 15:52 TMS Calc 1 BVJ0487 <br /> -- _ - --------- .._.----- ---- <br /> 4 EPA-300.0 10/03/12 10/03/12 20:12 LS1 IC2 1 BVJ0294 <br /> 5 EPA-150.1 10/05/12 10/05/12 12:54 RML META 1 BVJ0437 <br /> 6 EPA-120.1 10/05/12 10/05/12 12:54 RML MET-1 1 BVJ0437 <br /> 7 EPA-160.1 10/05/12 10/05/12 09:25 NW1 MANUAL 2 BVJ0445 <br /> 8 Calc 10/05/12 10/15/12 15:53 TMS Calc 1 BVJ0487 <br /> - -- 9 EPA-351.2- ---- 10/12/12 10/15/12 11:09 SDU SC-1 1 BVJ1086 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party BC Laboratories,Inc.assumes no responsibility for report alteration separation,detachment or third party interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 46 of 60 <br />