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ME Laboratories, Inc. . ,, <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107.03 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> Quality Control Report - Laboratory Control Sample <br /> Control Limits <br /> Spike Percent Percent Lab <br /> Constituent QC Sample ID Type Result Level Units Recovery RPD Recovery RPD Qualls <br /> QC Batch ID: BVJ0293 <br /> Chloride BVJ0293-BS1 LCS 50.214 50.000 mg/L 100 90-110 <br /> Nitrate as N BVJ0293-BS1 LCS 4.9590 5.0000 mg/L 99.2 90-110 _ <br /> Sulfate BVJ0293-BS1 LCS 100.89 100.00 mg/L 101 90-110 <br /> QC Batch ID: BVJ0294 <br /> Chloride BVJ0294-BS1 LCS 50.469 50.000 mg/L 101 90-110 <br /> Nitrate as IN BVJ0294-BS1 LCS f 4.9830 5.0000 mg/L 99.7 90-110 <br /> Sulfate BVJ0294-BS1 LCS 101.75 100.00 mg/L 102 90-110 <br /> QC Batch ID: BVJ0435 <br /> pH BVJ0435-BS2 LCS 4.0200 4.0000 pH Units 100 -95-105 <br /> Electrical Conductivity Q 25 C BVJ0435-BS1 LCS 305.70 303.00 umhos/cm 101 90-110 <br /> QC Batch ID: BVJ0436 <br /> pH BVJ0436-BS2 LCS 4.0200 4.0000 pH Units 100 95-106 <br /> Electrical Conductivity @ 25 C BVJ0436-BS1 LCS 306.90 303.00 umhoslcm 101 90-110 <br /> QC Batch ID: BVJ0437 <br /> pH BVJ0437-BS2 LCS 4.0200 4.0000 pH Units 100 95-105 <br /> Electrical Conductivity @ 25 C BVJ0437-BS1 LCS 307.10 303.00 umhoslcm 101 90-110 <br /> QC Batch ID: BVJ0444 <br /> Total Dissolved Solids @ 180 C BVJ0444-BS1 LCS 575.00 586.00 mg/L 98.1 90-110 <br /> QC Batch ID: BVJ0445 <br /> Total Dissolved Solids aQ 180 C BVJ0445-BS1 LCS 595.00 586.00 mg/L 102 90-110 <br /> QC Batch ID: 13VJ0505 <br /> Dissolved Calcium BVJ0505-BS1 LCS 10.170 10.000 mg/L 102 85-116 _ <br /> Dissolved Magnesium BVJ0505-BS1 LCS 10.126 10.000 mg/L _101_ 85-116 <br /> Dissolved Sodium BVJ0505-BS1 _LCS 9.8047 10.000 mglL _98.0 85-115 <br /> Dissolved Potassium BVJ0505-BS1 LCS 9.6648 10.000 mg/L 96.6 86-115 <br /> QC Batch ID: BVJ0506 <br /> Dissolved Calcium BVJ0506-BS1 LCS 10.371 10.000 mg/L 104 85-115 <br /> Dissolved Magnesium _ BVJ0506-BS1 LCS 10.305 10.000 - mg/L 103 85-115 <br /> Dissolved Sodium BVJ0506-BS1 LCS 9.9929 10.000 mg/L 99.9 85-115 <br /> Dissolved Potassium BVJ0506-BS1 LCS 9.8020 10.000 mg/L 98.0 85-115 <br /> QC Batch ID: BVJ1085 <br /> Total Kjeldahl Nitrogen BVJ1085-BS1 LCS 1.9783 2.0000 mg/L 98.9 85-115 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party BC Laboratorics,Inc.assumes no responsibility for report alteratiorl separation,detachment or third party interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.belabs.com Page 52 of 60 <br />