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1.11Laboratories, Inc. P <br /> -M . <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/18/2012 15:24 <br /> 3590 Iron Court Project: Diamond Pet Foods <br /> Shasta Lake City, CA 96019 Project Number: 010107.03 <br /> Project Manager: David Kirk <br /> Water Analysis (Metals) <br /> Quality Control Report - Precision & Accuracy <br /> Control Limits <br /> Source Source Spike Percent Percent Lab <br /> Constituent Type Sample ID Result Result Added Units RPD Recovery RPD RecoveryQuals <br /> QC Batch ID: BVJ0505 Used client sample: Y- Description: OB-1, 10/02/2012 10:07 <br /> Dissolved Boron DUP 1218782-01 0.31435 0.30592 mg1L 2.7 20 <br /> MS 1218782-01 0.31435 1.3845 1.0204 mglL 105 85-115 <br /> MSD 1218782-01 0.31435 1.3884 1.0204 mglL 0.3 105 20 85-115 <br /> Dissolved Manganese DUP 1218782-01 ND yVND -- mg/L - 41 _- 20 <br /> MS 1218782-01 ND 0.52509 0.51020 mg1L 103 85-115 <br /> MSD 1218782-01 ND 0.52036 0.51020 mg1L 0.9 102 20 86-115 <br /> QC Batch ID: BVJ0506 Used client sample: Y- Description: 013-22, 10/02/2012 11:35 <br /> Dissolved Boron DUP 1218782-11 0.14700 0.14978 mglL 1.9 20 <br /> MS 1218782-11 0.14700 1.1891 1.0204 mglL 102 86-115 <br /> MSD 1218782-11 0.14700 1.2050 1.0204 mg1L 1.3 104 20 86-116 <br /> Dissolved Manganese DUP 1218782-11 0.25146 0.25407 mglL 1.0 20 <br /> MS 1218782-11 0.25146 0.77972 0.51020 mg1L 104 86-115 <br /> MSD 1218782-11 0.25146 0.78637 0.51020 mg1L 0.8 105 20 86-115 <br /> The results in this report apply to the samples analwed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party BC Laboratories,Inc.assumes no responsibility for report alteration separation,detachment or third party interpretation <br /> 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 59 of 60 <br />