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QC Sample Results C <br /> Client: Safety-Kleen Systems, Inc TestAmerica Job ID: 440-140711-1 <br /> Project/Site: O'Reilly <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) <br /> Lab Sample ID: MB 440-317006/1-A Client Sample ID: Method Blank <br /> Matrix: Solid Prep Type: TCLP <br /> Analysis Batch: 317202 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Benzene ND 0.020 mg/L 03/14/16 09:59 1 <br /> Carbon tetrachloride ND 0.050 mg/L 03/14/16 09:59 1 <br /> Chloroform ND 0.020 mg/L 03/14/16 09:59 1 <br /> 1,1-Dichloroethene ND 0.050 mg/L 03/14/16 09:59 1 <br /> 1,2-Dichloroethane ND 0.020 mg/L 03/14/16 09:59 1 • <br /> 2-Butanone(MEK) ND 0.10 mg/L 03/14/16 09:59 1 <br /> Tetrachloroethene ND 0.020 mg/L 03/14/16 09:59 1 <br /> Trichloroethene ND 0.020 mg/L 03/14/16 09:59 1 <br /> Vinyl chloride ND 0.050 mg/L 03/14/16 09:59 1 <br /> Chlorobenzene ND 0.020 mg/L 03/14/16 09:59 1 <br /> 1,4-Dichlorobenzene ND 0.020 mg/L 03/14/16 09:59 1 <br /> Hexachlorobutadiene ND 0.050 mg/L 03/14/16 09:59 1 <br /> MB MB <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac ❑ <br /> Toluene-d8(Surr) 107 80-124 03/14/16 09:59 1 <br /> 4-Bromofluorobenzene(Surr) 96 80-120 03/14/16 09:59 1 <br /> Dibromofluoromethane(Surr) 115 79-125 03/14/16 09:59 1 <br /> Lab Sample ID: LCS 440-317006/2-A Client Sample ID: Lab Control Sample <br /> Matrix: Solid Prep Type: TCLP <br /> Analysis Batch: 317202 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Benzene 0.250 0.243 mg/L 97 70-120 <br /> Carbon tetrachloride 0.250 0.245 mg/L 98 65-140 <br /> Chloroform 0.250 0.243 mg/L 97 70-130 <br /> 1,1-Dichloroethene 0.250 0.238 mg/L 95 70-125 <br /> 1,2-Dichloroethane 0.250 0.236 mg/L 94 60-140 <br /> 2-Butanone(MEK) 0.313 0.273 mg/L 87 40-140 <br /> Tetrachloroethene 0.250 0.259 mg/L 104 70-125 <br /> Trichloroethene 0.250 0.250 mg/L 100 70-125 <br /> Vinyl chloride 0.250 0.258 mg/L 103 55-135 <br /> Chlorobenzene 0.250 0.244 mg/L 97 75-120 <br /> 1,4-Dichlorobenzene 0.250 0.249 mg/L 100 75-120 <br /> Hexachlorobutadiene 0.250 0.254 mg/L 102 65-135 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 104 80-124 <br /> 4-Bromofluorobenzene(Surr) 99 80-120 <br /> Dibromofluoromethane(Surr) 105 79-125 <br /> Lab Sample ID: 440-140711-1 MS Client Sample ID: Brake Shaving <br /> Matrix: Solid Prep Type: TCLP <br /> Analysis Batch: 317202 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Benzene ND 0.250 0.255 mg/L 102 65-125 <br /> TestAmerica Irvine <br /> Page 9 of 22 3/15/2016 <br />