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Quality Control Results <br />Job Number: 720-922-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/21/2005 1248 <br />12/21/2005 1315 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3311 <br />1.0 <br />1.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Column ID: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Column ID: <br />Client Matrix:Solid <br />Analysis Batch: 720-3455 <br />Analysis Batch: 720-3455 <br />12/20/2005 1323 <br />12/20/2005 1323 <br />Prep Batch: 720-3311 <br />Prep Batch: 720-3311 <br />30.04 g <br />5 mL <br />PRIMARY <br />30.01 g <br />5 mL <br />PRIMARY <br />Method: 8015B <br />Preparation: 3550B <br />N/A <br />N/A <br />Varian DRO1 <br />Varian DRO1 <br />720-922-7 <br />720-922-7 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />66 71 60 - 130 7 30Diesel Range Organics [C10-C28] <br />Surrogate MS % Rec MSD % Rec Acceptance Limits <br />o-Terphenyl 68 75 60 - 130 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 52 of 55