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Analytical Data <br />Client: Kennedy/Jenks Consultants Job Number: 720-993-1 <br />Client Sample ID: <br />Lab Sample ID:Date Sampled: <br />Date Received: <br />OU2-AOI7-S-1-0/0.5 <br />12/13/2005 1131 <br />12/13/2005 1705Client Matrix:Solid <br />8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) <br />720-993-6 <br />Date Prepared: <br />Date Analyzed: <br />Dilution: <br />Preparation: <br />Method: <br />12/16/2005 1549 <br />12/19/2005 1637 <br />10 <br />8270C Analysis Batch: 720-3248 <br />Prep Batch: 720-3184 <br />Injection Volume: <br />Final Weight/Volume: <br />Initial Weight/Volume: <br />Lab File ID: <br />Instrument ID:Sat 2K2 <br />c:\saturnws\data\200512\12 <br />30.25 g <br />1 mL <br />3550B <br />Analyte Result (mg/Kg)RLQualifierDryWt Corrected: N <br />ND 1.74-Bromophenyl phenyl ether <br />ND 0.66Hexachlorobenzene <br />ND 3.3Pentachlorophenol <br />ND 0.66Phenanthrene <br />ND 0.66Anthracene <br />ND 1.7Di-n-butyl phthalate <br />ND 0.66Fluoranthene <br />ND 0.66Pyrene <br />ND 1.7Butyl benzyl phthalate <br />ND 1.73,3'-Dichlorobenzidine <br />ND 0.66Benzo[a]anthracene <br />ND 3.3Bis(2-ethylhexyl) phthalate <br />ND 0.66Chrysene <br />ND 1.7Di-n-octyl phthalate <br />ND 0.66Benzo[b]fluoranthene <br />ND 0.66Benzo[a]pyrene <br />ND 0.66Benzo[k]fluoranthene <br />ND *0.66Indeno[1,2,3-cd]pyrene <br />ND 0.66Benzo[g,h,i]perylene <br />ND 3.3Benzoic acid <br />ND 0.66Azobenzene <br />ND 6.6Dibenz(a,h)anthracene <br />Surrogate %Rec Acceptance Limits <br />44 23 - 120Nitrobenzene-d5 <br />60 30 - 1152-Fluorobiphenyl <br />75 18 - 137Terphenyl-d14 <br />46 25 - 1212-Fluorophenol <br />49 24 - 113Phenol-d5 <br />54 19 - 1222,4,6-Tribromophenol <br />STL San Francisco Page 30 of 141