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Analytical Data <br />Client: Kennedy/Jenks Consultants Job Number: 720-993-1 <br />Client Sample ID: <br />Lab Sample ID:Date Sampled: <br />Date Received: <br />OU2-AOI7-S-1-1/2 <br />12/13/2005 1131 <br />12/13/2005 1705Client Matrix:Solid <br />8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) <br />720-993-7 <br />Date Prepared: <br />Date Analyzed: <br />Dilution: <br />Preparation: <br />Method: <br />12/16/2005 1549 <br />12/19/2005 1706 <br />1.0 <br />8270C Analysis Batch: 720-3248 <br />Prep Batch: 720-3184 <br />Injection Volume: <br />Final Weight/Volume: <br />Initial Weight/Volume: <br />Lab File ID: <br />Instrument ID:Sat 2K2 <br />c:\saturnws\data\200512\12 <br />30.45 g <br />1 mL <br />3550B <br />Analyte Result (mg/Kg)RLQualifierDryWt Corrected: N <br />ND 0.174-Bromophenyl phenyl ether <br />ND 0.066Hexachlorobenzene <br />ND 0.33Pentachlorophenol <br />ND 0.066Phenanthrene <br />ND 0.066Anthracene <br />ND 0.17Di-n-butyl phthalate <br />ND 0.066Fluoranthene <br />ND 0.066Pyrene <br />ND 0.17Butyl benzyl phthalate <br />ND 0.173,3'-Dichlorobenzidine <br />ND 0.066Benzo[a]anthracene <br />ND 0.33Bis(2-ethylhexyl) phthalate <br />ND 0.066Chrysene <br />ND 0.17Di-n-octyl phthalate <br />ND 0.066Benzo[b]fluoranthene <br />ND 0.066Benzo[a]pyrene <br />ND 0.066Benzo[k]fluoranthene <br />ND *0.066Indeno[1,2,3-cd]pyrene <br />ND 0.066Benzo[g,h,i]perylene <br />ND 0.33Benzoic acid <br />ND 0.066Azobenzene <br />ND 0.66Dibenz(a,h)anthracene <br />Surrogate %Rec Acceptance Limits <br />67 23 - 120Nitrobenzene-d5 <br />69 30 - 1152-Fluorobiphenyl <br />73 18 - 137Terphenyl-d14 <br />69 25 - 1212-Fluorophenol <br />71 24 - 113Phenol-d5 <br />81 19 - 1222,4,6-Tribromophenol <br />STL San Francisco Page 32 of 141