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Quality Control Results <br />Job Number: 720-993-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/19/2005 1540 <br />12/19/2005 1609 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3184 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />12/16/2005 1549 <br />Prep Batch: 720-3184 <br />Analysis Batch: 720-3248 <br />c:\saturnws\data\200512\121905 <br />30.15 g <br />1 mL <br />c:\saturnws\data\200512\121905\ <br />30.18 g <br />1 mL <br />mg/Kg <br />12/16/2005 1549 <br />Analysis Batch: 720-3248 <br />Prep Batch: 720-3184 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K2 <br />Sat 2K2 <br />LCS 720-3184/2-A <br />LCSD 720-3184/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />7382 5 - 112 12 35Phenol <br />7784 12 - 158 8 35Bis(2-chloroethyl)ether <br />7279 23 - 134 9 352-Chlorophenol <br />6876 9 - 172 11 351,3-Dichlorobenzene <br />7082 20 - 124 17 351,4-Dichlorobenzene <br />7783 10 - 130 9 35Benzyl alcohol <br />6479 32 - 129 21 351,2-Dichlorobenzene <br />7383 10 - 130 14 352-Methylphenol <br />131157 10 - 130 18 35 **4-Methylphenol <br />7383 9 - 230 13 35N-Nitrosodi-n-propylamine <br />6780 40 - 113 19 35Hexachloroethane <br />7674 35 - 180 3 35Nitrobenzene <br />7877 21 - 196 0 35Isophorone <br />7574 29 - 182 2 352-Nitrophenol <br />7171 32 - 119 1 352,4-Dimethylphenol <br />7880 33 - 184 2 35Bis(2-chloroethoxy)methane <br />7374 10 - 130 2 352,4-Dichlorophenol <br />7879 44 - 142 1 351,2,4-Trichlorobenzene <br />7471 21 - 133 4 35Naphthalene <br />2733 10 - 130 20 354-Chloroaniline <br />6965 24 - 116 6 35Hexachlorobutadiene <br />7378 10 - 130 8 354-Chloro-3-methylphenol <br />7673 10 - 130 5 352-Methylnaphthalene <br />8180 10 - 130 2 35Hexachlorocyclopentadiene <br />7376 37 - 144 5 352,4,6-Trichlorophenol <br />7981 10 - 130 2 352,4,5-Trichlorophenol <br />7781 10 - 130 5 352-Chloronaphthalene <br />8079 10 - 130 1 352-Nitroaniline <br />9293 9 - 112 1 35Dimethyl phthalate <br />8692 33 - 145 8 35Acenaphthylene <br />7173 10 - 130 3 353-Nitroaniline <br />7884 47 - 145 8 35Acenaphthene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 116 of 141