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Analytical Data <br />Client: Kennedy/Jenks Consultants Job Number: 720-1027-1 <br />Client Sample ID: <br />Lab Sample ID:Date Sampled: <br />Date Received: <br />OU2-AOI4-S-1-5.3/6.3 <br />12/14/2005 0819 <br />12/14/2005 1740Client Matrix:Solid <br />8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) <br />720-1027-3 <br />Date Prepared: <br />Date Analyzed: <br />Dilution: <br />Preparation: <br />Method: <br />12/19/2005 1237 <br />12/21/2005 1331 <br />10 <br />8270C Analysis Batch: 720-3368 <br />Prep Batch: 720-3247 <br />Injection Volume: <br />Final Weight/Volume: <br />Initial Weight/Volume: <br />Lab File ID: <br />Instrument ID:Sat 2K1 <br />d:\data\200512\122105\720- <br />30.39 g <br />5 mL <br />3550B <br />Analyte Result (mg/Kg)RLQualifierDryWt Corrected: N <br />ND 8.44-Bromophenyl phenyl ether <br />ND 3.3Hexachlorobenzene <br />ND 16Pentachlorophenol <br />ND 3.3Phenanthrene <br />ND 3.3Anthracene <br />ND 8.4Di-n-butyl phthalate <br />ND 3.3Fluoranthene <br />ND 3.3Pyrene <br />ND 8.4Butyl benzyl phthalate <br />ND 8.43,3'-Dichlorobenzidine <br />ND 3.3Benzo[a]anthracene <br />ND 16Bis(2-ethylhexyl) phthalate <br />ND 3.3Chrysene <br />ND 8.4Di-n-octyl phthalate <br />ND 3.3Benzo[b]fluoranthene <br />ND 3.3Benzo[a]pyrene <br />ND 3.3Benzo[k]fluoranthene <br />ND 3.3Indeno[1,2,3-cd]pyrene <br />ND 3.3Benzo[g,h,i]perylene <br />ND 16Benzoic acid <br />ND 3.3Azobenzene <br />ND 33Dibenz(a,h)anthracene <br />Surrogate %Rec Acceptance Limits <br />30 23 - 120Nitrobenzene-d5 <br />110 30 - 1152-Fluorobiphenyl <br />0 18 - 137*Terphenyl-d14 <br />47 25 - 1212-Fluorophenol <br />14 24 - 113*Phenol-d5 <br />65 19 - 1222,4,6-Tribromophenol <br />STL San Francisco Page 93 of 347