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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/20/2005 0910 <br />12/20/2005 0937 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3247 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />12/19/2005 1237 <br />Prep Batch: 720-3247 <br />Analysis Batch: 720-3357 <br />d:\data\200512\122005\LCS <br />30.13 g <br />1 mL <br />d:\data\200512\122005\LCSD <br />30.19 g <br />1 mL <br />mg/Kg <br />12/19/2005 1237 <br />Analysis Batch: 720-3357 <br />Prep Batch: 720-3247 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />LCS 720-3247/2-A <br />LCSD 720-3247/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />8170 9 - 191 15 352,4-Dinitrophenol <br />9488 10 - 130 6 354-Nitrophenol <br />99 10 - 130 4 35 **Dibenzofuran <br />9586 39 - 139 9 352,4-Dinitrotoluene <br />10596 50 - 158 9 352,6-Dinitrotoluene <br />102103 9 - 114 2 35Diethyl phthalate <br />10296 25 - 158 6 354-Chlorophenyl phenyl ether <br />10386 59 - 121 18 35Fluorene <br />9386 10 - 130 8 354-Nitroaniline <br />7679 9 - 181 4 352-Methyl-4,6-dinitrophenol <br />8697 10 - 130 13 35N-Nitrosodiphenylamine <br />8895 53 - 127 8 354-Bromophenyl phenyl ether <br />7790 9 - 152 16 35Hexachlorobenzene <br />8287 14 - 176 5 35Pentachlorophenol <br />9291 10 - 130 1 35Phenanthrene <br />9084 27 - 133 7 35Anthracene <br />8894 10 - 130 6 35Di-n-butyl phthalate <br />8788 26 - 137 1 35Fluoranthene <br />107112 52 - 115 5 35Pyrene <br />101105 10 - 130 4 35Butyl benzyl phthalate <br />6972 10 - 130 5 353,3'-Dichlorobenzidine <br />9497 33 - 143 3 35Benzo[a]anthracene <br />93100 8 - 158 7 35Bis(2-ethylhexyl) phthalate <br />92105 17 - 168 13 35Chrysene <br />98100 4 - 146 2 35Di-n-octyl phthalate <br />9084 24 - 159 7 35Benzo[b]fluoranthene <br />9090 17 - 163 0 35Benzo[a]pyrene <br />9190 11 - 162 2 35Benzo[k]fluoranthene <br />9693 9 - 171 2 35Indeno[1,2,3-cd]pyrene <br />9799 9 - 219 3 35Benzo[g,h,i]perylene <br />3532 10 - 130 11 35Benzoic acid <br />9086 10 - 130 4 35Azobenzene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 304 of 347