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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/21/2005 1621 <br />12/21/2005 1651 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3247 <br />1.0 <br />10 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3368 <br />Analysis Batch: 720-3368 <br />12/19/2005 1237 <br />12/19/2005 1237 <br />Prep Batch: 720-3247 <br />Prep Batch: 720-3247 <br />d:\data\200512\122105\720-1 <br />30.40 g <br />1 mL <br />d:\data\200512\122105\720-10 <br />30.32 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1027-14 <br />720-1027-14 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />51 52 5 - 112 1 35Phenol <br />67 65 12 - 158 3 35Bis(2-chloroethyl)ether <br />57 58 23 - 134 2 352-Chlorophenol <br />64 65 9 - 172 1 351,3-Dichlorobenzene <br />63 64 20 - 124 2 351,4-Dichlorobenzene <br />64 50 10 - 130 24 35Benzyl alcohol <br />64 71 32 - 129 10 351,2-Dichlorobenzene <br />40 41 10 - 130 3 352-Methylphenol <br />89 91 10 - 130 3 354-Methylphenol <br />64 57 9 - 230 11 35N-Nitrosodi-n-propylamine <br />62 64 40 - 113 3 35Hexachloroethane <br />74 75 35 - 180 1 35Nitrobenzene <br />77 84 21 - 196 10 35Isophorone <br />65 54 29 - 182 18 352-Nitrophenol <br />30 35 32 - 119 15 35 *2,4-Dimethylphenol <br />75 72 33 - 184 3 35Bis(2-chloroethoxy)methane <br />71 76 10 - 130 7 352,4-Dichlorophenol <br />72 79 44 - 142 10 351,2,4-Trichlorobenzene <br />68 78 21 - 133 13 35Naphthalene <br />41 38 10 - 130 9 354-Chloroaniline <br />69 74 24 - 116 8 35Hexachlorobutadiene <br />71 76 10 - 130 6 354-Chloro-3-methylphenol <br />79 82 10 - 130 4 352-Methylnaphthalene <br />46 41 10 - 130 11 35Hexachlorocyclopentadiene <br />67 72 37 - 144 8 352,4,6-Trichlorophenol <br />78 81 10 - 130 4 352,4,5-Trichlorophenol <br />77 90 10 - 130 16 352-Chloronaphthalene <br />78 87 10 - 130 11 352-Nitroaniline <br />85 93 9 - 112 9 35Dimethyl phthalate <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 306 of 347