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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/21/2005 1621 <br />12/21/2005 1651 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3247 <br />1.0 <br />10 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3368 <br />Analysis Batch: 720-3368 <br />12/19/2005 1237 <br />12/19/2005 1237 <br />Prep Batch: 720-3247 <br />Prep Batch: 720-3247 <br />d:\data\200512\122105\720-1 <br />30.40 g <br />1 mL <br />d:\data\200512\122105\720-10 <br />30.32 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1027-14 <br />720-1027-14 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />82 82 17 - 163 1 35Benzo[a]pyrene <br />72 77 11 - 162 8 35Benzo[k]fluoranthene <br />70 80 9 - 171 13 35Indeno[1,2,3-cd]pyrene <br />72 78 9 - 219 7 35Benzo[g,h,i]perylene <br />6 1 10 - 130 NC 35 **Benzoic acid <br />77 80 10 - 130 4 35Azobenzene <br />74 83 10 - 130 NC 35Dibenz(a,h)anthracene <br />Surrogate MS % Rec MSD % Rec Acceptance Limits <br />Nitrobenzene-d5 66 65 23 - 120 <br />2-Fluorobiphenyl 71 92 30 - 115 <br />Terphenyl-d14 82 78 18 - 137 <br />2-Fluorophenol 41 40 25 - 121 <br />Phenol-d5 49 47 24 - 113 <br />2,4,6-Tribromophenol 52 50 19 - 122 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 308 of 347