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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/26/2005 1033 <br />12/26/2005 1101 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3494 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />12/23/2005 1159 <br />Prep Batch: 720-3494 <br />Analysis Batch: 720-3536 <br />d:\data\200512\122605\LCS <br />30.28 g <br />1 mL <br />d:\data\200512\122605\LCSD <br />30.21 g <br />1 mL <br />mg/Kg <br />12/23/2005 1159 <br />Analysis Batch: 720-3536 <br />Prep Batch: 720-3494 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />LCS 720-3494/2-A <br />LCSD 720-3494/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />8277 9 - 191 7 352,4-Dinitrophenol <br />8888 10 - 130 0 354-Nitrophenol <br />870 10 - 130 199 35 **Dibenzofuran <br />9086 39 - 139 4 352,4-Dinitrotoluene <br />8991 50 - 158 2 352,6-Dinitrotoluene <br />9993 9 - 114 6 35Diethyl phthalate <br />9893 25 - 158 6 354-Chlorophenyl phenyl ether <br />8686 59 - 121 0 35Fluorene <br />9098 10 - 130 8 354-Nitroaniline <br />9294 9 - 181 2 352-Methyl-4,6-dinitrophenol <br />9192 10 - 130 1 35N-Nitrosodiphenylamine <br />100103 53 - 127 3 354-Bromophenyl phenyl ether <br />8989 9 - 152 1 35Hexachlorobenzene <br />98106 14 - 176 8 35Pentachlorophenol <br />9399 10 - 130 6 35Phenanthrene <br />9493 27 - 133 2 35Anthracene <br />103103 10 - 130 0 35Di-n-butyl phthalate <br />9398 26 - 137 5 35Fluoranthene <br />94106 52 - 115 12 35Pyrene <br />9495 10 - 130 1 35Butyl benzyl phthalate <br />6575 10 - 130 14 353,3'-Dichlorobenzidine <br />85104 33 - 143 20 35Benzo[a]anthracene <br />84100 8 - 158 16 35Bis(2-ethylhexyl) phthalate <br />96112 17 - 168 16 35Chrysene <br />8399 4 - 146 17 35Di-n-octyl phthalate <br />9182 24 - 159 11 35Benzo[b]fluoranthene <br />8686 17 - 163 1 35Benzo[a]pyrene <br />7283 11 - 162 14 35Benzo[k]fluoranthene <br />9089 9 - 171 1 35Indeno[1,2,3-cd]pyrene <br />8988 9 - 219 1 35Benzo[g,h,i]perylene <br />2319 10 - 130 15 35Benzoic acid <br />9187 10 - 130 5 35Azobenzene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 320 of 347