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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/29/2005 0752 <br />12/29/2005 0758 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3593 <br />1.0 <br />1.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3735 <br />Analysis Batch: 720-3735 <br />12/27/2005 1728 <br />12/27/2005 1728 <br />Prep Batch: 720-3593 <br />Prep Batch: 720-3593 <br />1.00 g <br />50 mL <br />1.05 g <br />50 mL <br />Method: 6010B <br />Preparation: 3050B <br />N/A <br />N/A <br />Varian ICP <br />Varian ICP <br />720-1027-48 <br />720-1027-48 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />14 15 75 - 125 4 20 **Antimony <br />83 83 75 - 125 4 20Arsenic <br />63 48 75 - 125 7 20 **Barium <br />84 85 75 - 125 4 20Beryllium <br />81 82 75 - 125 4 20Cadmium <br />83 84 75 - 125 3 20Chromium <br />81 81 75 - 125 4 20Cobalt <br />87 94 75 - 125 2 20Copper <br />77 122 75 - 125 33 20 *Lead <br />65 64 75 - 125 7 20 **Molybdenum <br />81 84 75 - 125 1 20Nickel <br />79 81 75 - 125 3 20Selenium <br />87 88 75 - 125 4 20Silver <br />80 80 75 - 125 5 20Thallium <br />77 77 75 - 125 3 20Vanadium <br />77 95 75 - 125 10 20Zinc <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 337 of 347