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QA/QC Report for Metals Reference#: JLA 25083 Reporting units: ppm Matrix Spike(MS)/Matrix Spike Duplicate(MSD) 601013/7471A Laboratory Sample#: AZ12382-001 Date of Extraction: 03/30/20 14:00 MS Date MSD Date SPC % % ACP ACP Analyte of Analysis of Analysis R1 CONC MS MSD MS MSD RPD %MS RPD Qualifiers Antimony 03/31/20 16:26 03/31/20 16:29 0.00 20.0 3.42 2.81 17 14 20 75-125 20 M2, Arsenic 03/31/2016:26 03/31/2016:29 2.90 20.0 21.6 19.6 94 84 10 75-125 20 -- Barium 03/31/2016:26 03/31/2016:29 88.0 20.0 116 107 140 95 8 75-125 20 M3, Beryllium 03/31/2016:26 03/31/2016:29 0.76 20.0 18.2 17.4 87 83 4 75-125 20 -- Cadmium 03/31/2016:26 03/31/2016:29 0.00 20.0 17.5 16.8 88 84 4 75-125 20 -- Cobalt 03/31/20 16:26 03/31/20 16:29 9.30 20.0 27.7 26.3 92 85 5 75-125 20 -- Copper 03/31/2016:26 03/31/2016:29 20.0 20.0 41.6 38.9 108 95 7 75-125 20 -- Lead 03/31/20 16:26 03/31/20 16:29 16.0 20.0 33.3 31.4 86 77 6 75-125 20 -- Molybdenum 03/31/2016:26 03/31/2016:29 0.00 20.0 14.2 14.1 71 71 1 75-125 20 M2, Nickel 03/31/2016:26 03/31/2016:29 15.0 20.0 33.5 31.5 93 83 6 75-125 20 -- Selenium 03/31/2016:26 03/31/2016:29 0.00 20.0 16.6 16.0 83 80 4 75-125 20 -- Silver 03/31/2016:26 03/31/2016:29 0.00 20.0 16.0 15.3 80 77 4 75-125 20 -- Thallium 03/31/2016:26 03/31/2016:29 0.00 20.0 12.3 11.9 62 59 3 75-125 20 M2, Vanadium 03/31/2016:26 03/31/2016:29 30.0 20.0 48.7 46.6 94 83 4 75-125 20 -- Zinc 03/31/20 16:26 03/31/20 16:29 48.0 20.0 72.1 68.1 120 100 6 75-125 20 -- Laboratory Control Spike(LCS)/Laboratory Control Spike Duplicate(LCSD) 6010B17471A Laboratory Sample#: JV0330202 Date of Extraction: 03/30/20 14:00 LCS Date LCSD Date SPC % % ACP ACP Analyte of Analysis of Analysis CONC LCS LCSD LCS LCSD RPD %LCS RPD Qualifiers Antimony 03/31/20 16:13 03/31/20 16:16 20.0 20.4 20.2 102 101 1 80-120 20 -- Arsenic 03/31/2016:13 03/31/2016:16 20.0 18.8 18.3 94 91 3 80-120 20 -- Barium 03/31/2016:13 03/31/2016:16 20.0 18.0 18.2 90 91 1 80-120 20 -- Beryllium 03/31/2016:13 03/31/2016:16 20.0 19.0 19.0 95 95 0 80-120 20 -- Cadmium 03/31/2016:13 03/31/2016:16 20.0 18.9 19.1 94 96 1 80-120 20 -- Cobalt 03/31/20 16:13 03/31/20 16:16 20.0 20.9 21.0 104 105 0 80-120 20 -- Copper 03/31/2016:13 03/31/2016:16 20.0 19.7 19.9 99 99 1 80-120 20 -- Lead 03/31/20 16:13 03/31/20 16:16 20.0 19.0 19.2 95 96 1 80-120 20 -- Molybdenum 03/31/2016:13 03/31/2016:16 20.0 18.0 18.1 90 91 1 80-120 20 -- Nickel 03/31/2016:13 03/31/2016:16 20.0 20.5 20.5 102 102 0 80-120 20 -- Selenium 03/31/2016:13 03/31/2016:16 20.0 19.1 18.8 96 94 2 80-120 20 -- Silver 03/31/2016:13 03/31/2016:16 20.0 17.4 17.6 87 88 1 80-120 20 -- Thallium 03/31/2016:13 03/31/2016:16 20.0 19.1 19.3 96 96 1 80-120 20 -- Vanadium 03/31/2016:13 03/31/2016:16 -- 20.0 18.3 18.4 91 92 1 80-120 20 -- Zinc 03/31/20 16:13 03/31/20 16:16 -- 20.0 18.6 18.4 93 92 1 80-120 20 -- Matrix Spike (MS)/Matrix Spike Duplicate(MSD) 6010B17471A Laboratory Sample#: 25088-001 Date of Extraction: 04/02/20 12:00 MS Date MSD Date SPC % % ACP ACP Analyte of Analysis of Analysis R1 CONC MS MSD MS MSD RPD %MS RPD Qualifiers Mercury 04/06/2016:46 04/06/2016:48 0.00 1.00 0.811 0.747 81 75 8 75-125 20 M2, Laboratory Control Spike(LCS)/Laboratory Control Spike Duplicate(LCSD) 601013/7471A Laboratory Sample#: JV0402204 Date of Extraction: 04/02/20 12:00 LCS Date LCSD Date SPC % % ACP ACP Analyte of Analysis of Analysis CONC LCS LCSD LCS LCSD RPD %LCS RPD Qualifiers Mercury 04/06/2016:41 04/06/2016:43 -- 1.00 1.05 1.05 105 105 0 80-120 20 -- @ Orange Coast Analytical, Inc 6 of 8 Rev1.0 04/09/20