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GeoAnalytical Laboratories, Inc. ' 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 CERTIFICATE OF ANALYSIS ' Report# L181-15 Oxygenates Date 7/10/00 Date Recd 6/29/00 WHF Environmental Project Raymond Greer Date Started 7/06/00 ' PO Box 427 15634 5temegul Rd Escalon Date Completed 7/10/00 Oakdale CA 95361 PO# Date Sampled 6/28/00 ' Sampler Sample ID Lab ID RL Method Analyte Results Units MW-9-50 L21950 10 8260B Methyl tertiary-Butyl Ether (MTBE) ND pg/Kg 100 Ethanol ND pg/Kg 100 tertiary-Butanol ND pg/Kg 10 Di-isopropyl ether(DIPE) ND pg/Kg 10 Ethyl tertiary-Butyl Ether (ETBE) ND pg/Kg 10 tertiary-Amyl Methyl Ether (TAME) ND pg/Kg MW-9-75 L21951 10 8260B Methyl tertiary-Butyl Ether (MTBE) ND pg/Kg 100 Ethanol ND pg/Kg 100 tertiary-Butanol ND pg/Kg 10 Di-isopropyl ether(DIPE) ND pg/Kg 10 Ethyl tertiary-Butyl Ether (ETBE) ND pg/Kg 10 tertiary-Amyl Methyl Ether(TAME) ND pg/Kg MW-9-90 L21952 10 8260B Methyl tertiary-Butyl Ether (MTBE) ND p /K Ypg/Kg 100 Ethanol ND pg/Kg 100 tertiary-Butanol ND pg/Kg 10 Di-isopropyl ether(DIPE) ND pg/Kg 10 Ethyl tertiary-Butyl Ether (ETBE) ND pg/Kg 10 tertiary-Amyl Methyl Ether(TAME) ND pg/Kg B-104-70 L21953 10 8260B Methyl tertiary-Butyl Ether (MTBE) ND pg/Kg I 100 Ethanol ND pg/Kg 100 tertiary-Butanol ND pg/Kg 10 Di-isopropyl ether(DIPE) ND pg/Kg 10 Ethyl tertiary-Butyl Ether (ETBE) ND pg/Kg 10 tertiary-Amyl Methyl Ether (TAME) ND pg/Kg Diluted due to high level of non-target analytes B-104-90 L21954 10 8260B Methyl tertiary-Butyl Ether (MTBE) ND pg/Kg 100 Ethanol ND pg/Kg 100 tertiary-Butanol ND pg/Kg 10 Di-isopropyl ether(DIPE) ND pg/Kg 10 Ethyl tertiary-Butyl Ether (ETBE) ND pg/Kg 10 tertiary-Amyl Methyl Ether(TAME) ND gg/Kg IMario D'Onofrlo Donna Keller Chemist Certification # 1157 Laboratory Director