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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone:925-798-1620 Fax:925-798-1622 <br /> . 4- Website:www.mccampbell.com E-mail:main(a mccampbell.com <br /> Geophase Environmental Client Project ID: #474.2;Haley Date Sampled: 05/12/06 <br /> 2937 Venernan Ave., Suite B240 <br /> Date Received: 05/12/06 <br /> Client Contact: Steve Lankford Date Extracted 05/12/06 <br /> Modesto,CA 95356 Client P.O.: G1197 Date Analyzed 05/18/06 <br /> Organochlorine Pesticides by GC-ECD(8080 Basic Target List)* <br /> Extraction Method:SW3510C Analytical Method:SW8081B Work Order:0605256 <br /> Lab ID 0605256-OOIA 0605256-002A 0605256-003A 0605256-004A <br /> Reporting Limit for <br /> Client ID 133 [34 B5 B6 DF=1 <br /> Matrix W W W W <br /> DF -- I l - I 10 S W <br /> Com ound Concentration pg/kg pg/L <br /> Aldrin ND ND ND ND<0.050 NA 0.005 <br /> a-BHC ND ND ND ND<O.10 NA 0.01 <br /> -b-BHC ND ND ND ND<0.050 NA 0.005 <br /> -d-BHC - ND ND ND ND<0.050 NA 0.005 <br /> BHC ND ND ND ND<0.20 NA 0.02 <br /> Chlordane Technical ND ND ND ND<1.0 NA 0.1 <br /> a-Chlordane ND ND ND ND<0.50 NA 0.05 <br /> -Chlordane -- ND ND ND ND<0.50 NA 0.05 <br /> -DDD ND ND NDND<0.10 NA 0.01 <br /> p,p-DDE ND ND NDND<0.10 NA 0.01 <br /> p,p-DDT ND ND ND ND<0.50 NA 0.05 <br /> Dieldrin ND ND ND ND<0.10 NA 0.01 <br /> Endosulfan I ND ND ND 1.2 NA 0.02 <br /> Endosulfan II ND ND ND 0.84 NA 0.01 <br /> Endosulfan sulfate 0.096 ND ND 2.3 NA 0.05 <br /> Endrin ND ND ND 1.0 NA 0.01 <br /> Endrin aldehyde ND ND ND ND<O.10 NA 0.01 <br /> Heptachlor ND ND ND ND<0.10 NA 0.01 <br /> Heptachlor epoxide ND ND ND ND<0.10 NA 0.01 <br /> Methoxychlor ND ND ND N6<1.0 NA 0.1 <br /> Toxaphene ND ND 1.7 22 NA 0.5 <br /> Surro ate Recoveries <br /> %SS: 99 104 104 84 <br /> Comments i i i i <br /> *water samples in gg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,filter samples in pg/filter,product/oil/non-aqueous liquid samples <br /> and all TCLP&SPLP extracts are reported in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> (a)PCB aroclor 1016;(b)PCB aroclor 1221;(c)PCB aroclor 1232;(d)PCB aroclor 1242;(e)PCB aroclor 1248;(f)PCB aroclor 1254;(g)PCB aroclor <br /> 1260;(h)a lighter than water immiscible sheen/product is present;(i)liquid sample that contains>-1 vol.%sediment;(j)sample diluted due to high <br /> organic content/matrix interference;(k)p,p,-is the same as 4,4,-; (1)florisil(EPA 3620)cleanup;(m)silica-gel(EPA 3630)cleanup;(n)elemental sulfur <br /> EPA 3660 cleanup; o sulfuric acid permanganate EPA 3665 cleanup; r results are reported on a dry weight basis; see attached narrative. <br /> DHS Certification No. 16444_ ,___�ngela Rydelius, Lab Manager <br />