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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone:925-798-1620 Fax:925-798-1622 <br /> Z4 1 Website:www.niccampbell.com E-mail:main@niccampbell.com <br /> Geophase Environmental Client Project ID: #474.2;Haley Date Sampled: 05/12/06 <br /> 2937 Veneman Ave., Suite B240 <br /> Date Received: 05/12/06 <br /> Client Contact: Steve Lankford Date Extracted 05/12/06 <br /> Modesto, CA 95356 Client P.O.: G1197 Date Analyzed 05/18/06 <br /> Organochlorine Pesticides by GC-ECD(8080 Basic Target List)* <br /> Extraction Method:SW3510C Analytical Method:SW808113 Work Order:0605256 <br /> Lab ID 0605256-009A 0605256-OIOA <br /> -- - — - _ Reporting Limit for <br /> Client ID Eq Blank Decom DF=1 <br /> Matrix W W <br /> DF I 5 S W <br /> Com pound Concentration µg/kg µg/L <br /> Aldrin ND ND<0.025 NA 0.005 <br /> a-BHC ND ND<0.050 NA 0.01 <br /> b-BHC ND ND<0.025 NA 0.005 <br /> -d-BHC ND ND<0.025 NA 0.005 <br /> -BHC ND ND<0.10 NA 0.02 <br /> Chlordane(Technical) ND ND<0.50 NA 0.1 <br /> a-Chlordane ND ND<0.25 NA 0.05 <br /> Chlordane ND ND<0.25 NA 0.05 <br /> -DDD ND ND<0.050 NA 0.01 <br /> p,p-DDE ND ND<0.050 NA 0.01 <br /> p,p-DDT ND ND<0.25 NA 0.05 <br /> Dieldrin ND ND<0.050 NA 0.01 <br /> Endosulfan[ ND 1.4 NA 0.02 <br /> Endosulfan II ND 0.75 NA 0.01 <br /> Endosulfan sulfate ND ND<0.25 NA 0.05 <br /> Endrin ND ND<0.050 NA 0.01 <br /> Endrin aldehyde ND ND<0.050 NA 0.01 <br /> Heptachlor ND ND<0.050 I NA 0.01 <br /> -Heptachlor epoxide ND ND<0.050 NA 0.01 <br /> -Methoxychlor ND ND<0.50 4NA 0.1 <br /> Toxaphene Nn ND<2.5 NA 0.5 <br /> Surro ate Recoveries <br /> %SS: 104 94 <br /> Comments <br /> *water samples inµg/L,soil/sludge/solid samples in mg/kg,wipe samples inµg/wipe,filter samples inµg/filter,prod uct/oiI/non-aqueous liquid samples <br /> and all TCLP&SPLP extracts are reported in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> (a)PCB aroclor 1016;(b)PCB aroclor 1221;(c)PCB aroclor 1232;(d)PCB aroclor 1242;(e)PCB aroclor 1248;(f)PCB aroclor 1254;(g)PCB aroclor <br /> 1260;(h)a lighter than water immiscible sheen/product is present;(i)liquid sample that contains>-1 vol.%sediment;0)sample diluted due to high <br /> organic content/matrix interference;(k)p,p,-is the same as 4,4,-; (1)florisil(EPA 3620)cleanup;(m)silica-gel(EPA 3630)cleanup;(n)elemental sulfur <br /> EPA 3660 cleanup; o sulfuric acid permanganate EPA 3665 cleanup; r results are reported on a dry weight basis; see attached narrative. <br /> DHS Certification No. 1644 Angela Rydelius, Lab Manager <br />