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I110 2nd Avenue South ND7 Pacheen CA 94553 5560 <br /> McCampbell Analytical Incj Telephone 925-798 1620 Fax 925-798-1622 <br /> http Ilwww mccampbell com E mad mamQinccampbell corn <br /> QC SUMMARY REPORT FOR SW8260B <br /> I <br /> Matrix W WorkOrder 0208114 <br /> EPA Method SW82606 Extraction SW5030B BatchlD 3359 Spiked Sample ID 0208114-002C <br /> Sam le I MS* MSD' MS-MSD" LCs LCSD ILCS-LCSD Acceptance Criteria <br /> � (%) <br /> Compound —_ - -- — - - - — -�- -- <br /> N %Rec %Rec ` % RPD %Rec % Rec %RPD Low High <br /> gIL Jgj�tent-Amyl methyl ether(TAME) ND 10 921 981 631 109 121 101 I 70 130 <br /> Methyl-t-butyl ether(MTBC) ND 10 92 94 7 295 108 120 106 70 130 <br />' Diisopropyl ether(DIPE) ND 10 984 100 2 09 109 117 677 70 130 <br /> — I -- <br /> Ethyl Cert-butyl ether(ETBE) ND 10 101 103 2 09 114 126 1 977 70 130 <br />' %SSI ND 1 100 826 828 0 214 985 100 177-- <br /> 70 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> I NONE <br />�s <br /> t <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent <br />' Deviation <br /> N/A=not enough sample to perform matrix spike and matrix spice duplicate <br /> NR=analyte concentration in sample exceeds spike amount for sod matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or <br /> analyte content <br />' %Recovery=100"(MS-Sample)I(Amount Spiked) RPD=100'(MS—MSD)1(MS+MSD)"2 <br /> "MS and/or MSD spike recoveries may not be near 100%or the RPDs near 0%if a)the sample is inhomogenous AND contains significant concentrations of <br />' analyte relative to the amount spiked orb)if that specific sample matrix interferes with spike recovery <br />