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819 Striker Avenue,Suite 8 <br /> Sequoia Sacramento,CA 95834 <br /> (916)921-9600 <br /> i!DFAX(916)921-0100 <br /> II&V Analytical www.sequoialabs.com <br /> Kleinfelder-Stockton Project: Mel Rice Terminal S405100 <br /> 2825 East Myrtle Street.. Project Number: 43851.E01 Reported: <br /> Stockton CA,95205 Project Manager: Doug Heard 05/25/04 16:45 <br /> Conventional Chemistry Parameters by APHA/EPA Methods - Quality Control <br /> Sequoia Analytical- Petaluma <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 4050467-General Preparation <br /> Laboratory Control Sample(4050467-BSI) Prepared:05/19/04 Analyzed:05/20/04 <br /> Total Kjeldahl Nitrogen 173 20 mg/kg 200 86 80-120 <br /> Matrix Spike(4050467-MSI) Source:S405100-04 Prepared:05/19/04 Analyzed:05/20/04 <br /> Total Kjeldahl Nitrogen 599 20 mg/kg 200 390 104 75-125 <br /> Matrix Spike Dup(4050467-MSDI) Source: 5405100-04 Prepared:05/19/04 Analyzed:05/20/04 <br /> Total Kjeldahl Nitrogen 595 20 mg/kg 200 390 102 75-125 0.7 35 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 17 of 23 <br />