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Client Sample Results C Client:Antea USA, Inc. TestAmerica Job ID: 720-41618-1 Project/Site: UPRR-Stockton Client Sample ID: B15-1.0-1.5 Lab Sample ID: 720-41618-18 Date Collected:04/12/12 15:45 Matrix: Solid Date Received:04/17/12 18:09 Method: 82608/CA_LUFTMS-8260B/CA LUFT MS(Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Toluene ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 1,2,3-Trichlorobenzene ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 1,2,4-Trichlorobenzene ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 1,1,1-Trichloroethane ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 1,1,2-Trichloroethane ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 Trichloroethene ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 Trichlorofluoromethane ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 1,2,3-Trichloropropane ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 1,2,4-Trimethylbenzene ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 1,3,5-Trimethylbenzene ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 Vinyl acetate ND 45 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 Vinyl chloride ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 Xylenes,Total ND 8.9 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 2,2-Dichloropropane ND 4.5 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 Gasoline Range Organics(GRO) ND 220 ug/Kg 04/19/12 15:00 04/19/12 23:39 1 -C5-C12 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-BromoFluorobenzene 90 45-131 04/19/12 15:00 04/19/12 23.39 1 1,2-Dichloroethane-d4(Surr) 113 60-140 04/19/12 15:00 04/19/12 23:39 1 Toluene-0(Surr) 95 58-140 04/19/12 15:00 04/19/12 23:39 1 Method: 8270C SIM-PAHs by GCMS(SIM) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Acenaphthylene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Anthracene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Benzo[a]anthracene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Benzo[a]pyrene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Benzo[b]fluoranthene 5.1 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Benzo[g,h,i]perylene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Benzo[k]fluoranthene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Chrysene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Dibenz(a,h)anthracene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Fluoranthene 6.6 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Fluorene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Indeno[1,2,3-cd]pyrene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Naphthalene ND 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Phenanthrene 7.0 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Pyrene 5.7 5.0 ug/Kg 04/19/1216:49 04/20/1215:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 2-Fluorobiphenyl 80 33-120 04/19112 16:49 04/20112 15:53 1 Terphenyl-04 82 35-146 04/19112 16:49 04/20112 15:53 1 Method: 8015B-Diesel Range Organics(DRO)(GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Diesel Range Organics[C10-C28] 23 0.99 mg/Kg 04/19/12 10:36 04/20/12 16:04 1 Motor Oil Range Organics[C24-C36] ND 50 mg/Kg 04/19/12 10:36 04/20/12 16:04 1 TestAmerica Pleasanton Page 43 of 145 4/26/2012