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Client Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-41618-1 <br /> Project/Site: UPRR-Stockton <br /> Client Sample ID: 137-1.0-1.5 Lab Sample ID: 720-41618-19 <br /> Date Collected: 04/13/12 08:00 Matrix: Solid <br /> Date Received: 04/17/12 18:09 <br /> Method: 82608/CA_LUFTMS-8260B/CA LUFT MS(Continued) <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Toluene ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,2,3-Trichlorobenzene ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,2,4-Trichlorobenzene ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,1,1-Trichloroethane ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,1,2-Trichloroethane ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> Trichloroethene ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> Trichlorofluoromethane ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,2,3-Trichloropropane ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,2,4-Trimethylbenzene 180 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,3,5-Trimethylbenzene 69 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> Vinyl acetate ND 48 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> Vinyl chloride ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> Xylenes,Total ND 9.6 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> 2,2-Dichloropropane ND 4.8 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> Gasoline Range Organics(GRO) 1700 240 ug/Kg 04/24/12 18:58 04/24/12 23:29 1 <br /> -C5-C12 <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> 4-Bromofluorobenzene 75 45-131 04/24/12 18:58 04/24/12 23:29 1 <br /> 1,2-Dichloroethane-d4(Surr) 113 60-140 04/24/12 18:58 04/24/12 23:29 1 <br /> Toluene-d8(Surr) 84 58-140 04/24/12 18:58 04/24/12 23:29 1 <br /> Method: 8270C SIM-PAHs by GCMS(SIM) <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Acenaphthene ND 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Acenaphthylene ND 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Anthracene ND 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Benzo[a]anthracene 120 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Benzo[a]pyrene ND 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Benzo[b]fluoranthene 360 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Benzo[g,h,i]perylene ND 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Benzo[k]fluoranthene 340 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Chrysene 570 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Dibenz(a,h)anthracene ND 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Fluoranthene 290 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Fluorene 200 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Indeno[1,2,3-cd]pyrene ND 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Naphthalene 210 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Phenanthrene 680 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Pyrene 280 50 ug/Kg 04/19/1216:49 04/20/1218:15 5 <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> 2-Fluorobiphenyl 70 33-120 04/19/12 16:49 04/20/12 18:15 5 <br /> Terphenyl-d14 77 35-146 04/19/12 16:49 04/20/12 18:15 5 <br /> Method: 80158-Diesel Range Organics(DRO)(GC) <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Diesel Range Organics[C10-C28] 2300 100 mg/Kg 04/19/12 10:36 04/23/12 17:15 100 <br /> Motor Oil Range Organics 17000 5000 mg/Kg 04/19/12 10:36 04/23/12 17:15 100 <br /> [C24-C36] <br /> TestAmerica Pleasanton <br /> Page 47 of 145 4/26/2012 <br />