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QC Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-41618-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 8260B/CA_LUFTMS - 8260B/CA LOFT MS (Continued) <br /> Lab Sample ID:720-41618-1 MS Client Sample ID: B11-2.0-2.5 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 112064 Prep Batch: 112098 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichloroethane-d4(Surr) 99 60-140 <br /> Toluene-d8(Surr) 96 58-140 <br /> Lab Sample ID: 720-41618-1 MSD Client Sample ID: B11-2.0-2.5 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 112064 Prep Batch: 112098 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Methyl tert-butyl ether ND 47.5 45.6 ug/Kg 96 69-130 0.000 20 <br /> Acetone ND 238 197 ug/Kg 83 37-150 10.9 20 <br /> Benzene ND 47.5 47.3 ug/Kg 100 70-130 1.00 20 <br /> Dichlorobromomethane ND 47.5 50.6 ug/Kg 106 64-135 1.00 20 <br /> Bromobenzene ND 47.5 46.2 ug/Kg 97 70-130 1.43 20 <br /> Chlorobromomethane ND 47.5 47.7 ug/Kg 100 65-130 0.000 20 <br /> Bromoform ND 47.5 48.5 ug/Kg 102 58-132 1.00 20 <br /> Bromomethane ND 47.5 39.2 ug/Kg 82 56-130 0.000 20 <br /> 2-Butanone(MEK) ND 238 203 ug/Kg 85 41-150 9.10 20 <br /> n-Butylbenzene ND 47.5 52.7 ug/Kg 111 60-145 1.64 20 <br /> sec-Butylbenzene ND 47.5 52.7 ug/Kg 111 64-137 1.28 20 <br /> tert-Butylbenzene ND 47.5 52.5 ug/Kg 110 63-134 2.02 20 <br /> Carbon disulfide ND 47.5 49.2 ug/Kg 104 10-150 0.000 20 <br /> Carbon tetrachloride ND 47.5 50.8 ug/Kg 107 54-130 1.00 20 <br /> Chlorobenzene ND 47.5 45.8 ug/Kg 96 70-130 3.14 20 <br /> Chloroethane ND 47.5 43.0 ug/Kg 90 61-130 2.88 20 <br /> Chloroform ND 47.5 47.3 ug/Kg 100 67-130 1.81 20 <br /> Chloromethane ND 47.5 42.2 ug/Kg 89 50-131 6.70 20 <br /> 2-Chlorotoluene ND 47.5 52.3 ug/Kg 110 70-130 1.00 20 <br /> 4-Chlorotoluene ND 47.5 50.4 ug/Kg 106 70-130 0.000 20 <br /> Chlorodibromomethane ND 47.5 49.0 ug/Kg 103 60-141 0.000 20 <br /> 1,2-Dichlorobenzene ND 47.5 44.3 ug/Kg 93 70-130 0.000 20 <br /> 1,3-Dichlorobenzene ND 47.5 46.2 ug/Kg 97 70-130 1.00 20 <br /> 1,4-Dichlorobenzene ND 47.5 44.9 ug/Kg 94 70-130 0.000 20 <br /> 1,3-Dichloropropane ND 47.5 46.6 ug/Kg 98 70-130 1.43 20 <br /> 1,1-Dichloropropene ND 47.5 49.2 ug/Kg 104 67-130 1.35 20 <br /> 1,2-Dibromo-3-Chloropropane ND 47.5 45.6 ug/Kg 96 57-130 1.87 20 <br /> Ethylene Dibromide ND 47.5 47.0 ug/Kg 99 66-135 2.60 20 <br /> Dibromomethane ND 47.5 45.8 ug/Kg 96 65-131 2.27 20 <br /> Dichlorodifluoromethane ND 47.5 35.6 ug/Kg 75 38-130 0.000 20 <br /> 1,1-Dichloroethane ND 47.5 49.4 ug/Kg 104 67-130 1.74 20 <br /> 1,2-Dichloroethane ND 47.5 45.2 ug/Kg 95 70-130 1.48 20 <br /> 1,1-Dichloroethene ND 47.5 47.0 ug/Kg 99 64-130 2.23 20 <br /> cis-1,2-Dichloroethene ND 47.5 55.7 ug/Kg 117 68-131 1.00 20 <br /> trans-1,2-Dichloroethene ND 47.5 39.9 ug/Kg 84 70-130 1.00 20 <br /> 1,2-Dichloropropane ND 47.5 48.1 ug/Kg 101 65-133 1.00 20 <br /> cis-1,3-Dichloropropene ND 47.5 50.4 ug/Kg 106 46-139 0.000 20 <br /> trans-1,3-Dichloropropene ND 47.5 53.8 ug/Kg 113 55-131 0.000 20 <br /> Ethylbenzene ND 47.5 48.1 ug/Kg 101 65-130 1.38 20 <br /> Hexachlorobutadiene ND 47.5 41.6 ug/Kg 88 58-132 8.27 20 <br /> 2-Hexanone ND 238 213 ug/Kg 90 44-150 5.61 20 <br /> TestAmerica Pleasanton <br /> Page 89 of 145 4/26/2012 <br />