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QC Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-41618-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 8260B/CA_LUFTMS - 8260B/CA LOFT MS (Continued) <br /> Lab Sample ID:720-41618-4 MSD Client Sample ID: 138-1.5-2.0 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 112352 Prep Batch: 112356 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D °/Rec Limits RPD Limit <br /> Dibromomethane ND 49.3 52.1 ug/Kg 106 65-131 4 20 <br /> Dichlorodifluoromethane ND 49.3 37.1 ug/Kg 75 38-130 3 20 <br /> 1,1-Dichloroethane ND 49.3 53.1 ug/Kg 108 67-130 2 20 <br /> 1,2-Dichloroethane ND 49.3 52.7 ug/Kg 107 70-130 5 20 <br /> 1,1-Dichloroethene ND 49.3 47.7 ug/Kg 97 64-130 2 20 <br /> cis-1,2-Dichloroethene ND 49.3 56.4 ug/Kg 114 68-131 1 20 <br /> trans-1,2-Dichloroethene ND 49.3 42.2 ug/Kg 86 70-130 1 20 <br /> 1,2-Dichloropropane ND 49.3 56.4 ug/Kg 114 65-133 2 20 <br /> cis-1,3-Dichloropropene ND 49.3 54.8 ug/Kg 111 46-139 2 20 <br /> trans-1,3-Dichloropropene ND 49.3 48.5 ug/Kg 98 55-131 2 20 <br /> Ethylbenzene ND 49.3 50.9 ug/Kg 103 65-130 1 20 <br /> Hexachlorobutadiene ND 49.3 31.4 ug/Kg 64 58-132 6 20 <br /> 2-Hexanone ND 247 252 ug/Kg 102 44-150 15 20 <br /> Isopropyl benzene ND 49.3 54.2 ug/Kg 110 65-130 1 20 <br /> 4-Isopropyltoluene ND 49.3 57.6 ug/Kg 117 69-134 4 20 <br /> Methylene Chloride ND 49.3 54.4 ug/Kg 104 63-130 7 20 <br /> 4-Methyl-2-pentanone(MIBK) ND 247 298 ug/Kg 121 51-140 15 20 <br /> Naphthalene ND 49.3 28.2 ug/Kg 57 45-146 16 20 <br /> N-Propylbenzene ND 49.3 60.7 ug/Kg 123 70-130 5 20 <br /> Styrene ND 49.3 52.5 ug/Kg 106 58-135 3 20 <br /> 1,1,1,2-Tetrachloroethane ND 49.3 58.6 ug/Kg 119 64-133 4 20 <br /> 1,1,2,2-Tetrachloroethane ND 49.3 71.2 F ug/Kg 144 70-131 17 20 <br /> Tetrachloroethene ND 49.3 48.3 ug/Kg 98 67-130 1 20 <br /> Toluene ND 49.3 51.1 ug/Kg 104 70-130 1 20 <br /> 1,2,3-Trichlorobenzene ND 49.3 26.4 F ug/Kg 54 58-138 13 20 <br /> 1,2,4-Trichlorobenzene ND 49.3 28.4 ug/Kg 58 49-144 14 20 <br /> 1,1,1-Trichloroethane ND 49.3 53.5 ug/Kg 108 57-133 2 20 <br /> 1,1,2-Trichloroethane ND 49.3 56.8 ug/Kg 115 68-132 6 20 <br /> Trichloroethene ND 49.3 49.3 ug/Kg 100 66-130 1 20 <br /> Trichlorofluoromethane ND 49.3 51.9 ug/Kg 105 61-130 3 20 <br /> 1,2,3-Trichloropropane ND 49.3 72.4 ug/Kg 147 62-150 20 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 49.3 55.0 ug/Kg 112 52-130 4 20 <br /> ne <br /> 1,2,4-Trimethylbenzene ND 49.3 60.7 ug/Kg 123 64-140 5 20 <br /> 1,3,5-Trimethylbenzene ND 49.3 63.7 ug/Kg 129 67-134 6 20 <br /> Vinyl acetate ND 49.3 55.2 ug/Kg 112 52-150 6 20 <br /> Vinyl chloride ND 49.3 49.7 ug/Kg 101 62-130 1 20 <br /> m-Xylene&p-Xylene ND 98.6 105 ug/Kg 106 70-130 0 20 <br /> o-Xylene ND 49.3 54.2 ug/Kg 110 68-130 1 20 <br /> 2,2-Dichloropropane ND 49.3 51.5 ug/Kg 104 63-130 2 20 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 95 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 108 60-140 <br /> Toluene-d8(Surr) 103 58-140 <br /> TestAmerica Pleasanton <br /> Page 99 of 145 4/26/2012 <br />