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QC Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-41618-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 8270C SIM - PAHs by GCMS (SIM) (Continued) <br /> Lab Sample ID: 720-41618-31 MS Client Sample ID: 133-1.0-1.5 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 112128 Prep Batch: 112082 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Acenaphthene ND 332 230 ug/Kg 69 33-120 <br /> Acenaphthylene ND 332 258 ug/Kg 78 28-120 <br /> Anthracene ND 332 254 ug/Kg 76 36-120 <br /> Benzo[a]anthracene ND 332 232 ug/Kg 70 29-120 <br /> Benzo[a]pyrene ND 332 259 ug/Kg 77 24-120 <br /> Benzo[b]fluoranthene ND 332 265 ug/Kg 79 17-132 <br /> Benzo[g,h,i]perylene ND 332 204 ug/Kg 61 21-120 <br /> Benzo[k]fluoranthene ND 332 263 ug/Kg 79 35-120 <br /> Chrysene ND 332 239 ug/Kg 72 29-120 <br /> Dibenz(a,h)anthracene ND 332 236 ug/Kg 71 36-120 <br /> Fluoranthene ND 332 251 ug/Kg 74 24-120 <br /> Fluorene ND 332 245 ug/Kg 74 35-120 <br /> Indeno[1,2,3-cd]pyrene ND 332 225 ug/Kg 68 20-126 <br /> Naphthalene 6.4 332 217 ug/Kg 63 32-120 <br /> Phenanthrene 5.6 332 242 ug/Kg 71 28-120 <br /> Pyrene 5.4 332 258 ug/Kg 76 24-123 El <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 2-Fluorobiphenyl 81 33-120 <br /> Terphenyl-d14 86 35-146 <br /> FLab Sample ID: 720-41618-31 MSD Client Sample ID: 133-1.0-1.5 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 112128 Prep Batch: 112082 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Acenaphthene ND 332 238 ug/Kg 72 33-120 3.59 20 <br /> Acenaphthylene ND 332 260 ug/Kg 78 28-120 1.05 20 <br /> Anthracene ND 332 259 ug/Kg 78 36-120 2.23 20 <br /> Benzo[a]anthracene ND 332 241 ug/Kg 73 29-120 3.97 20 <br /> Benzo[a]pyrene ND 332 265 ug/Kg 79 24-120 2.18 20 <br /> Benzo[b]fluoranthene ND 332 272 ug/Kg 81 17-132 2.87 20 <br /> Benzo[g,h,i]perylene ND 332 205 ug/Kg 62 21-120 1.00 20 <br /> Benzo[k]fluoranthene ND 332 276 ug/Kg 83 35-120 4.71 20 <br /> Chrysene ND 332 251 ug/Kg 76 29-120 4.78 20 <br /> Dibenz(a,h)anthracene ND 332 237 ug/Kg 71 36-120 0.000 20 <br /> Fluoranthene ND 332 263 ug/Kg 78 24-120 4.82 20 <br /> Fluorene ND 332 252 ug/Kg 76 35-120 2.71 20 <br /> Indeno[1,2,3-cd]pyrene ND 332 226 ug/Kg 68 20-126 0.000 20 <br /> Naphthalene 6.4 332 232 ug/Kg 68 32-120 6.71 20 <br /> Phenanthrene 5.6 332 255 ug/Kg 75 28-120 5.25 20 <br /> Pyrene 5.4 332 274 ug/Kg 81 24-123 5.77 20 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> 2-Fluorobiphenyl 84 33-120 <br /> Terphenyl-d14 89 35-146 <br /> TestAmerica Pleasanton <br /> Page 103 of 145 4/26/2012 <br />