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QC Sample Results C Client:Antea USA, Inc. TestAmerica Job ID: 720-41618-1 Project/Site: UPRR-Stockton Method: 60108 - Metals (ICP) (Continued) FLab Sample ID: 720-41618-1 MSD Client Sample ID: B11-2.0-2.5 Matrix: Solid Prep Type:Total/NA Analysis Batch: 112102 Prep Batch: 112044 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Antimony ND 48.5 21.3 F mg/Kg 42 75-125 3.82 20 Arsenic 5.5 48.5 48.9 mg/Kg 89 75-125 4.10 20 Barium 140 48.5 170 F mg/Kg 70 75-125 7.98 20 Beryllium ND 48.5 47.0 mg/Kg 97 75-125 4.33 20 Cadmium ND 48.5 45.5 mg/Kg 94 75-125 4.65 20 Chromium 35 48.5 82.0 mg/Kg 97 75-125 0.000 20 Cobalt 13 48.5 59.1 mg/Kg 96 75-125 5.72 20 Copper 27 48.5 71.7 mg/Kg 92 75-125 1.00 20 Lead 21 48.5 55.0 F mg/Kg 70 75-125 1.00 20 Molybdenum ND 48.5 42.6 mg/Kg 86 75-125 4.33 20 Nickel 27 48.5 73.3 mg/Kg 94 75-125 3.79 20 Selenium ND 48.5 42.5 mg/Kg 88 75-125 3.32 20 Silver ND 24.3 23.3 mg/Kg 96 75-125 2.98 20 Thallium ND 48.5 46.1 mg/Kg 95 75-125 4.42 20 Vanadium 46 48.5 90.5 mg/Kg 92 75-125 2.90 20 Zinc 36 48.5 80.0 mg/Kg 90 75-125 1.30 20 Lab Sample ID: MB 720-112120/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type:Total/NA Analysis Batch: 112191 Prep Batch: 112120 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 0.50 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Arsenic ND 1.0 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Barium ND 0.50 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Beryllium ND 0.10 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Cadmium ND 0.13 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Chromium ND 0.50 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Cobalt ND 0.20 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Copper ND 1.5 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Lead ND 0.50 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Molybdenum ND 0.50 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Nickel ND 0.50 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Selenium ND 1.0 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Silver ND 0.25 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Thallium ND 0.50 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Vanadium ND 0.50 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Zinc ND 1.5 mg/Kg 04/20/12 07:48 04/20/12 19:57 1 Lab Sample ID: LCS 720-112120/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type:Total/NA Analysis Batch: 112191 Prep Batch: 112120 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Antimony 50.0 49.5 mg/Kg 99 80-120 Arsenic 50.0 50.6 mg/Kg 101 80-120 Barium 50.0 51.7 mg/Kg 103 80-120 Beryllium 50.0 51.1 mg/Kg 102 80-120 Cadmium 50.0 49.8 mg/Kg 100 80-120 Chromium 50.0 50.8 mg/Kg 102 80-120 TestAmerica Pleasanton Page 112 of 145 4/26/2012