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Client Sample Results C Client:Antea USA, Inc. TestAmerica Job ID: 720-41618-1 Project/Site: UPRR-Stockton Client Sample ID: 139-1.0-1.5 Lab Sample ID: 720-41618-3 Date Collected: 04/12/12 13:45 Matrix: Solid Date Received: 04/17/12 18:09 Method: 82608/CA_LUFTMS-8260B/CA LUFT MS(Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Toluene ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 1,2,3-Trichlorobenzene ND 4.7 ug/Kg 04/19/1215:00 04/19/1221:17 1 1,2,4-Trichlorobenzene ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 1,1,1-Trichloroethane ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 1,1,2-Trichloroethane ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 Trichloroethene ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 Trichlorofluoromethane ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 1,2,3-Trichloropropane ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 1,2,4-Trimethylbenzene ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 1,3,5-Trimethylbenzene ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 Vinyl acetate ND 47 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 Vinyl chloride ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 Xylenes,Total ND 9.4 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 2,2-Dichloropropane ND 4.7 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 Gasoline Range Organics(GRO) ND 240 ug/Kg 04/19/12 15:00 04/19/12 21:17 1 -C5-C12 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene 92 45-131 04/19/12 15:00 04/19/12 21:17 1 1,2-Dichloroethane-d4(Surr) 105 60-140 04/19/12 15:00 04/19/12 21:17 1 Toluene-d8(Surr) 98 58-140 04/19/12 15:00 04/19/12 21:17 1 Method: 8270C SIM-PAHs by GCMS(SIM) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Acenaphthylene ND 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Anthracene 7.9 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Benzo[a]anthracene 42 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Benzo[a]pyrene 47 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Benzo[b]fluoranthene 65 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Benzo[g,h,i]perylene 20 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Benzo[k]fluoranthene 20 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Chrysene 50 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Dibenz(a,h)anthracene 7.5 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Fluoranthene 79 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Fluorene ND 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Indeno[1,2,3-cd]pyrene 19 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Naphthalene 7.1 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Phenanthrene 36 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Pyrene 77 5.0 ug/Kg 04/19/1216:48 04/20/1217:28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2-Fluorobiphenyl 66 33-120 04/19/12 16:48 04/20/12 17:28 1 Terphenyl-d14 70 35-146 04/19/12 16:48 04/20/12 17:28 1 Method: 60108-Metals(ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony 2.8 2.0 mg/Kg 04/19/12 12:06 04/19/12 20:52 4 Arsenic 5.8 4.0 mg/Kg 04/19/12 12:06 04/19/12 20:52 4 Barium 110 2.0 mg/Kg 04/19/12 12:06 04/19/12 20:52 4 Beryllium ND 0.40 mg/Kg 04/19/12 12:06 04/19/12 20:52 4 TestAmerica Pleasanton Page 18 of 145 4/26/2012