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Client Sample Results C Client:Antea USA, Inc. TestAmerica Job ID: 720-41618-1 Project/Site: UPRR-Stockton Client Sample ID: 135-4-4.5 Lab Sample ID: 720-41618-12 Date Collected:04/12/12 11:08 Matrix: Solid Date Received:04/17/12 18:09 Method: 82608/CA_LUFTMS-8260B/CA LUFT MS(Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Toluene ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 1,2,3-Trichlorobenzene ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 1,2,4-Trichlorobenzene ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 1,1,1-Trichloroethane ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 1,1,2-Trichloroethane ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 Trichloroethene ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 Trichlorofluoromethane ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 1,2,3-Trichloropropane ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 1,2,4-Trimethylbenzene ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 1,3,5-Trimethylbenzene ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 Vinyl acetate ND 46 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 Vinyl chloride ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 Xylenes,Total ND 9.3 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 2,2-Dichloropropane ND 4.6 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 Gasoline Range Organics(GRO) ND 230 ug/Kg 04/19/12 15:00 04/19/12 22:42 1 -C5-C12 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-BromoFluorobenzene 94 45-131 04/19/12 15:00 04/19/12 22.42 1 1,2-Dichloroethane-d4(Surr) 111 60-140 04/19/12 15:00 04/19/12 22:42 1 Toluene-d8(Surr) 98 58-140 04/19/12 15:00 04/19/12 22:42 1 Method: 8270C SIM-PAHs by GCMS(SIM) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Acenaphthylene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Anthracene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Benzo[a]anthracene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Benzo[a]pyrene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Benzo[b]fluoranthene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Benzo[g,h,i]perylene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Benzo[k]fluoranthene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Chrysene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Dibenz(a,h)anthracene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Fluoranthene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Fluorene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Indeno[1,2,3-cd]pyrene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Naphthalene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Phenanthrene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Pyrene ND 5.0 ug/Kg 04/19/1216:48 04/20/1215:06 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2-Fluorobiphenyl 74 33-120 04/19112 16:48 04/20112 15:06 1 Terphenyl-04 81 35-146 04/19112 16:48 04/20112 15:06 1 Method: 80158-Diesel Range Organics(DRO)(GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Diesel Range Organics[C10-C28] 1.3 0.99 mg/Kg 04/19/12 10:36 04/20/12 17:15 1 Motor Oil Range Organics[C24-C36] ND 49 mg/Kg 04/19/12 10:36 04/20/12 17:15 1 TestAmerica Pleasanton Page 31 of 145 4/26/2012