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Gec ..,,nalytical Laboratories, nc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> Report# N072-21 CERTIFICATE OF ANALYSIS Date: 3/21/02 <br /> Oxygenates Date Rec'd: 3/13/02 <br /> Thorpe Oil Date Started: 3/19/02 <br /> PO Box 357 Project: Tank Pull-Prendor(Stockton) Date Completed:3/20/02 <br /> Lodi CA 95241 <br /> Date Sampled: 3/13/02_ <br /> PO# Time: <br /> Sample ID: Stockpile #1,2,3 Sampler : R Azevedo(Geo) <br /> Lab ID: N200673,N200674,N200675 <br /> Method RL. Analyte Results Units <br /> 8260B 10 Methyl tert-butyl ether (MTBE) ND pg/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> s <br /> Surrogate Amnt Spiked Amnt Rec %Recovery QC Limit% <br /> 1,2-Didloroethane-d4 100 117 117.0 66-133 <br /> 2-Bromo-l-chloropropane 100 104 104.0 63-139 <br /> 4-Bromofluorobenzene 100 102 102.0 64-136 <br /> IvL gg- Q� ZI/ I <br /> Mario D Onofrio <br /> Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />