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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Client Applied Earth Sciences, Incorporated Service Request X0400795 <br /> Project Canteen Corp/AGE-NC-99-0612 Date Collected 08/16/2004 <br /> mple Matrix Water Date Received 08/17/2004 <br /> IVolatile Organic Compounds <br /> ISample Name MW-1I/081604 Units uglL <br /> Lab Code X0400795-006 Basis NA <br /> Extraction Method EPA 5030B Level Low <br />' Analysis Method 8260B <br /> Dilution Date Date Extraction <br /> Analyte Name Result Q MRL MDL Factor Extracted Analyzed Lot Note <br /> Methyl tert-Butyl Ether 9 2 10 0 80 1 08/30/04 08/30/04 XWG0400953 <br /> Benzene ND U 0 50 0 30 1 08/30/04 08/30/04 XWG0400953 <br /> 1,2-Dichloroethane 96 D 50 50 10 09/13/04 09/13/04 XWG0400980 <br /> Toluene ND U 0 50 020 1 08/30/04 08/30/04 XWG0400953 <br /> 1,2-Dibromoethane ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> Ethylbenzene ND U 0 50 020 1 08/30/04 08/30/04 XWG0400953 <br /> m,p-Xylenes ND U 10 060 1 08/30/04 08/30/04 XWG0400953 <br /> o-Xylene ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> tert-Butyl Alcohol ND U 20 10 1 08/30/04 08/30/04 XWG0400953 <br /> Diisopropyl Ether ND U 10 040 1 08/30/04 08/30/04 XWG0400953 <br /> tert-Amyl Methyl Ether ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> tent-Butyl Ethyl Ether ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> We Case Narrative <br /> Control Date <br /> Surrogate Name %Rec Iamlt5 Analyzed Note <br /> Dibromofluoromethane 89 77-121 08/30/04 Acceptable <br /> Toluene-d8 84 65-131 08/30/04 Acceptable <br /> 4-Bromofluorobenzene 76 68-125 08/30/04 Acceptable <br /> Gents <br /> Printed 09/20/2004 11 5123 Form IA-Organic Page I of I <br /> 0 <br /> L 1STEALTH\CRYSTAL RPT\Formlm rpt Merged SuperSet Referent RR4937 <br />