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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> Client Applied Earth Sciences, Incorporated Service Request X0400795 <br /> Project: Canteen Corp/AGE-NC-99-0612 Date Extracted. 08/25/2004 <br /> *pie Matrix Water Date Analyzed 08/25/2004 <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> TPH as Gasoline(GRO) <br /> Sample Name. MW-13B/081604 Units ug/L <br /> Lab Code, X0400795-005 Basis. NA <br /> Extraction Method EPA 5030B Level Low <br /> Analysis Method 8015 GRO Extraction Lot. XWG0400905 <br /> MW-13B/081604MS MW-13B/081604DMS <br /> XWG0400905-1 XWG0400905-2 <br /> Sample Matrix Spike Duplicate Matrix Spike %Rec RPD <br />' Analyte Name Result Result Expected "/oRec Result Expected %Rec Limits RPD Limit <br /> C6-C10 GRO 32 1020 1000 99 1050 1000 102 70-130 3 20 <br /> f <br /> Wagged with an asterisk(•)indicate values outside control critena <br /> agged with a pound(#)indicate the contra[criteria is not applicable <br />' Percent rcowenes and mUbve percent dtffemnces(RPD)am determined by the software using values In the calculation wtuah haus not been rounded <br /> 1 Printed 08/27/2004 09 59 04 Form 3A-Organic Page I of 1 <br /> ZTEALMCRYSTAL RMFonn3DMS rpt SuperSet Reference RR4894 <br />