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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> Client Applied Earth Sciences, Inc Service Request X2400480 <br /> Project Canteen Corp Date Extracted 05/24/2004 <br /> Onple Matrix Water Date Analyzed 05/24/2004 <br /> Matrix Spike Summary <br /> TPH as Gasoline(GRO) <br /> Sample Name MW 13B Units tig/L <br /> Lab Code X2400480-007 Basis NA <br /> Extraction Method EPA 5030B Level Low <br /> Analysis Method 8015 GRO Extraction Lot XWG0400583 <br /> MW 13BMS <br /> XWG0400583-1 <br /> Sample Matrix Spike %Rec <br /> Analyte Name Result Result Expected %Rec Limits <br /> C6 -CIO GRO 64 907 1000 84 70-130 <br /> t <br /> Its flagged with an asterisk(•}indicate values outside control criteria <br />' Its flagged with a pound(#)indicate the control criteria is not applicable <br /> Percent recoveries and relative percent differences(RPT)are determined by the software using values in the calculation which have not been rounded <br />' Printed 05/30/2004 09 06 43 Form 3A-Organic Page 1 of I <br /> L 1STEALTMCRYSTAL RPTIFonn3MS rpt SuperSet Reference RR4623 <br />