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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Client- Applied Earth Sciences, Inc Service Request L2400620 <br /> P olect Canteen Date Collected 03/11/2004 <br /> ple Matrix Soil Date Received 03/12/2004 <br /> BTEX by 8021B <br /> Sample Name STK3 Units ug/Kg <br /> Lab Code- L2400620-003 Basis Wet <br /> Extraction Method EPA 5030B Level Low <br /> Analysis Method 8021B <br /> Dilution Date Date Extraction <br /> Analyte Name Result Q MRL Factor Extracted Analyzed Lot Note <br /> Benzene ND U 50 1 03/16/04 03/16/04 LWG0401116 <br /> Toluene ND U 50 1 03/16/04 03/16/04 LWG0401116 <br /> Ethylbenzene ND U 50 1 03/16/04 03/16/04 LWG0401116 <br /> Xylenes,Total ND U 15 1 03/16/04 03/16/04 LWG0401116 <br /> Control Date <br /> Surrogate Name %Rec Limits Analyzed Note <br /> 4-Bromofluorobenzene 74 43-127 03/16/04 Acceptable <br /> • <br /> WentS <br /> Printed 03/17/2004 17 24 13 Form 1 Z-Organic Page d of 1 <br /> P 1STEAL714ICRYSTAL RPTFomilm rpt Merged Superset Reference RR5312 <br />