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110 2nd Avenue South #D7 Pacheco CA 94553 5560 <br /> E4: <br /> MCCampbe71 Analytical IIIC Telephone 925-798 1620 Fax 925 798 1622 <br /> littp Ilwww mccarrilibell com E-mail mam�bell com <br /> A E S Regulatory Services Client Project ID Canteen Corp Date Sampled 05/27/03 <br /> 2013 Wells Branch Pkwy Ste 206 Date Received 05/28/03 <br /> Austin,TX 78728 Client Contact Paul Dotson Date Extracted 05/29/03-05/30/03 <br /> CIient P O Date.Analyzed 05/29/03-05/30/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW50309 Analytical Method SW8260B Work Order 0305421 <br /> Lab ID 0305421-OOIB 0305421-002B 0305421-003B 0305421-004B <br /> Client ID MW 3 MW 3A MW 3D MW 11 <br /> Reporting Limit for <br /> Matrix W W W W DF—f <br /> DF 5 10 1 5 S W <br /> Compound Concentration ug/kg pg/L <br /> tert Amyl methyl ether(TAME) ND<2 5 I ND<5 0 ND ND<2 5 NA 0 5 <br /> Benzene ND<2 5 ND<5 0 7 7 ND<2 5 NA _F0_5 <br /> t-Butyl alcohol(TBA) ND<25 ND<50 ND ND<25 NA 5 0 <br /> l,2-Dibromoethane(EDS) ND<2 5 ND<5 0 ND ND<2 5 NA 0 5 <br /> 1,2 Dichloroethane(1,2-DCA) ND<2 5 ND<5 0 ND 99 NA 0 5 <br /> Dusopropyl ether(DIPS) ND<2 5 ND<5 0 ND ND<2 5 NA 0 5 <br /> Ethylbenzene ND<2 5 ND<5 0 6 2 ND<2 5 NA 0 5 <br /> Ethyl tert butyl ether(ETBE) ND<2 5 ND<5 0 ND ND<2 5 NA 0 5 <br /> Methyl-t-butyl ether(MTBE) 97 270 14 14 NA 0 5 <br /> Toluene ND<2 5 ND<5 0 ND ND<2 5 NA 0 5 <br /> Xylenes 2 9 ND<5 0 i 2 2 ND<2 5 NA 0 5 <br /> Surrogate Recoveries{%) <br /> 94 7 � 961 101 TI�102 <br /> %SS2 102 101 102 102 <br /> %SS3 103 105 I 106 101 <br /> Comments <br /> f <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples inµg/kg, wipe samples in lig/wipe, <br /> prod uct/otl/nnn-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than--2 vol %sediment i)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />